Crystal structures of N-(trichloroacetyl)morpholine and 2,6-di(trichloroacetyl)cyclohexanone
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| 024 | 7 | 0 | |a 10.1524/zkri.218.6.440.20723 |2 doi |
| 035 | |a (NATIONALLICENCE)gruyter-10.1524/zkri.218.6.440.20723 | ||
| 245 | 0 | 0 | |a Crystal structures of N-(trichloroacetyl)morpholine and 2,6-di(trichloroacetyl)cyclohexanone |h [Elektronische Daten] |c [Süheyla Özbey, F. B. Kaynak, H. Şenöz, N. Tunoğlu] |
| 520 | 3 | |a The crystal and molecular structure of the title compounds have been determined by X-ray analysis (N-(trichloroacetyl)morpholine, C6H8Cl3NO2, P21/a, a = 9.869(1) Å, b = 12.287(1) Å, c = 16.060(1) Å, β = 98.773(7)°, Z = 8; 2,6-di(trichloroacetyl)cyclohexanone, C10H8Cl6O3, Pbca, a = 10.553(1) Å, b = 15.405(2) Å, c = 18.435(2) Å, Z = 4). The morpholine and cyclohexane rings of both compounds adopt the chair conformation. There are some intra- and intermolecular hydrogen bonds in the title compounds, so the crystal structures of them are stabilized by C—H...Cl and C—H...O intra- and inter molecular hydrogen bonds. | |
| 540 | |a © 2003 Oldenbourg Wissenschaftsverlag GmbH | ||
| 690 | 7 | |a Crystallography |2 nationallicence | |
| 690 | 7 | |a Inorganic chemistry |2 nationallicence | |
| 690 | 7 | |a Organic chemistry |2 nationallicence | |
| 700 | 1 | |a Özbey |D Süheyla |4 aut | |
| 700 | 1 | |a Kaynak |D F. B. |4 aut | |
| 700 | 1 | |a Şenöz |D H. |4 aut | |
| 700 | 1 | |a Tunoğlu |D N. |4 aut | |
| 773 | 0 | |t Zeitschrift für Kristallographie - Crystalline Materials |d De Gruyter Oldenbourg |g 218/6(2003-06-01), 440-444 |x 2194-4946 |q 218:6<440 |1 2003 |2 218 |o zkri | |
| 856 | 4 | 0 | |u https://doi.org/10.1524/zkri.218.6.440.20723 |q text/html |z Onlinezugriff via DOI |
| 908 | |D 1 |a research article |2 jats | ||
| 950 | |B NATIONALLICENCE |P 856 |E 40 |u https://doi.org/10.1524/zkri.218.6.440.20723 |q text/html |z Onlinezugriff via DOI | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Özbey |D Süheyla |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Kaynak |D F. B. |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Şenöz |D H. |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Tunoğlu |D N. |4 aut | ||
| 950 | |B NATIONALLICENCE |P 773 |E 0- |t Zeitschrift für Kristallographie - Crystalline Materials |d De Gruyter Oldenbourg |g 218/6(2003-06-01), 440-444 |x 2194-4946 |q 218:6<440 |1 2003 |2 218 |o zkri | ||
| 900 | 7 | |b CC0 |u http://creativecommons.org/publicdomain/zero/1.0 |2 nationallicence | |
| 898 | |a BK010053 |b XK010053 |c XK010000 | ||
| 949 | |B NATIONALLICENCE |F NATIONALLICENCE |b NL-gruyter | ||