caa a22 4500 378881825 CHVBK 20180305123433.0 cr unu---uuuuu 161128e20030601xx s 000 0 eng 10.1524/zkri.218.6.440.20723 doi (NATIONALLICENCE)gruyter-10.1524/zkri.218.6.440.20723 Crystal structures of N-(trichloroacetyl)morpholine and 2,6-di(trichloroacetyl)cyclohexanone [Elektronische Daten] [Süheyla Özbey, F. B. Kaynak, H. Şenöz, N. Tunoğlu] The crystal and molecular structure of the title compounds have been determined by X-ray analysis (N-(trichloroacetyl)morpholine, C6H8Cl3NO2, P21/a, a = 9.869(1) Å, b = 12.287(1) Å, c = 16.060(1) Å, β = 98.773(7)°, Z = 8; 2,6-di(trichloroacetyl)cyclohexanone, C10H8Cl6O3, Pbca, a = 10.553(1) Å, b = 15.405(2) Å, c = 18.435(2) Å, Z = 4). The morpholine and cyclohexane rings of both compounds adopt the chair conformation. There are some intra- and intermolecular hydrogen bonds in the title compounds, so the crystal structures of them are stabilized by C—H...Cl and C—H...O intra- and inter molecular hydrogen bonds. © 2003 Oldenbourg Wissenschaftsverlag GmbH Crystallography nationallicence Inorganic chemistry nationallicence Organic chemistry nationallicence Özbey Süheyla aut Kaynak F. B. aut Şenöz H. aut Tunoğlu N. aut Zeitschrift für Kristallographie - Crystalline Materials De Gruyter Oldenbourg 218/6(2003-06-01), 440-444 2194-4946 218:6<440 2003 218 zkri https://doi.org/10.1524/zkri.218.6.440.20723 text/html Onlinezugriff via DOI 1 research article jats NATIONALLICENCE 856 40 https://doi.org/10.1524/zkri.218.6.440.20723 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Özbey Süheyla aut NATIONALLICENCE 700 1- Kaynak F. B. aut NATIONALLICENCE 700 1- Şenöz H. aut NATIONALLICENCE 700 1- Tunoğlu N. aut NATIONALLICENCE 773 0- Zeitschrift für Kristallographie - Crystalline Materials De Gruyter Oldenbourg 218/6(2003-06-01), 440-444 2194-4946 218:6<440 2003 218 zkri CC0 http://creativecommons.org/publicdomain/zero/1.0 nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-gruyter