caa a22 4500 378903055 CHVBK 20180305123522.0 cr unu---uuuuu 161128e20041201xx s 000 0 eng 10.1515/epoly.2004.4.1.784 doi (NATIONALLICENCE)gruyter-10.1515/epoly.2004.4.1.784 Synthesis and characterization of novel polyamides based on tridecanedioic acid: Nylons 3 13, 5 13, 6 13, 7 13, 9 13, 10 13, 11 13 [Elektronische Daten] [Xiaowen Cui, Deyue Yan, Dan Xiao] Linear polyamides with high aliphatic content were prepared through step-heating melt polycondensation of tridecanedioic acid with various diamines. The synthesized polyamides were characterized comprehensively by means of IR, NMR and Raman spectroscopy. In addition, thermogravimetry, differential scanning calorimetry and dynamic mechanical analysis were used to investigate thermal properties of the obtained polyamides. It was found that melting and crystallization temperatures decrease as the aliphatic content increases. X-ray diffraction was applied to determine the crystal structures of the polyamides. © 2013 by Walter de Gruyter GmbH & Co. Cui Xiaowen College of Chemistry and Chemical Technology, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, P. R. China; Fax 086-021-54741297 aut Yan Deyue College of Chemistry and Chemical Technology, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, P. R. China; Fax 086-021-54741297 aut Xiao Dan College of Chemistry and Chemical Technology, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, P. R. China; Fax 086-021-54741297 aut e-Polymers De Gruyter 4/1(2004-12-01), 784-792 2197-4586 4:1<784 2004 4 epoly https://doi.org/10.1515/epoly.2004.4.1.784 text/html Onlinezugriff via DOI 1 research article jats NATIONALLICENCE 856 40 https://doi.org/10.1515/epoly.2004.4.1.784 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Cui Xiaowen College of Chemistry and Chemical Technology, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, P. R. China; Fax 086-021-54741297 aut NATIONALLICENCE 700 1- Yan Deyue College of Chemistry and Chemical Technology, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, P. R. China; Fax 086-021-54741297 aut NATIONALLICENCE 700 1- Xiao Dan College of Chemistry and Chemical Technology, Shanghai Jiao Tong University, 800 Dongchuan Road, Shanghai 200240, P. R. China; Fax 086-021-54741297 aut NATIONALLICENCE 773 0- e-Polymers De Gruyter 4/1(2004-12-01), 784-792 2197-4586 4:1<784 2004 4 epoly CC0 http://creativecommons.org/publicdomain/zero/1.0 nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-gruyter