caa a22 4500 378915770 CHVBK 20180305123552.0 cr unu---uuuuu 161128e20040801xx s 000 0 eng 10.1524/zkri.219.8.461.38328 doi (NATIONALLICENCE)gruyter-10.1524/zkri.219.8.461.38328 Katrusiak Andrzej Shadowing and absorption corrections of single-crystal high-pressure data [Elektronische Daten] [Andrzej Katrusiak] The effect of shadowing the sample crystal enclosed in the diamond-anvil high-pressure cell (DAC) by the gasket edges, i.e. by the walls of the high-pressure chamber, has been described for unrestricted data-collection procedures. A general vector formalism reveals new features of the shadowing and absorption corrections, depending on the primary beam-DAC-reflection configuration. The corrections apply to the data measured with conventional normal-beam-equatorial diffractometers, or with area-detectors. The simple vector approach optimizes computations and affords straightforward corrections of intensities. Feasibility of enhancing the resolution of numerical integration by applying fine grid divisions, has been discussed. © 2004 Oldenbourg Wissenschaftsverlag GmbH Crystallography nationallicence Inorganic chemistry nationallicence Organic chemistry nationallicence Zeitschrift für Kristallographie - Crystalline Materials De Gruyter Oldenbourg 219/8(2004-08-01), 461-467 2194-4946 219:8<461 2004 219 zkri https://doi.org/10.1524/zkri.219.8.461.38328 text/html Onlinezugriff via DOI 1 research article jats NATIONALLICENCE 856 40 https://doi.org/10.1524/zkri.219.8.461.38328 text/html Onlinezugriff via DOI NATIONALLICENCE 100 1- Katrusiak Andrzej NATIONALLICENCE 773 0- Zeitschrift für Kristallographie - Crystalline Materials De Gruyter Oldenbourg 219/8(2004-08-01), 461-467 2194-4946 219:8<461 2004 219 zkri CC0 http://creativecommons.org/publicdomain/zero/1.0 nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-gruyter