Structure and characterization of methyl (±)-1-(2-aminophenyl)-2-hydroxy-4-(4-methoxybenzoyl)-5-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1H-pyrrole-2-acetate
| LEADER | caa a22 4500 | ||
|---|---|---|---|
| 001 | 378943405 | ||
| 003 | CHVBK | ||
| 005 | 20180305123658.0 | ||
| 007 | cr unu---uuuuu | ||
| 008 | 161128e20040901xx s 000 0 eng | ||
| 024 | 7 | 0 | |a 10.1524/zkri.219.9.554.44037 |2 doi |
| 035 | |a (NATIONALLICENCE)gruyter-10.1524/zkri.219.9.554.44037 | ||
| 245 | 0 | 0 | |a Structure and characterization of methyl (±)-1-(2-aminophenyl)-2-hydroxy-4-(4-methoxybenzoyl)-5-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1H-pyrrole-2-acetate |h [Elektronische Daten] |c [Cengiz Arıcı, Dinçer Ülkü, S. Hakan Üngören, Mustafa Saçmacı, Yunus Akçamur] |
| 520 | 3 | |a The stoichiometry of 1 was derived from the results of elemental analysis, IR, 1H, 13C-NMR, UV-Vis and mass spectroscopic techniques. The structure derived from physico-chemical methods is consistent with that of the X-ray diffraction. The compound crystallizes in the triclinic system, space group P1̅, with a = 9.3895(12), b = 11.3759(11), c = 12.8077(14)Å, α = 103.290(3)° β = 98.110(4)°, γ = 105.545(3)°, V = 1252.4(2)Å3, Z = 2. The molecule has a non-planar configuration. The methoxy carbonylmethyl group exhibits an E-configuration. The crystal structure is stabilized by intermolecular C—H O, N—H O and O—H O contacts. | |
| 540 | |a © 2004 Oldenbourg Wissenschaftsverlag GmbH | ||
| 690 | 7 | |a Crystallography |2 nationallicence | |
| 690 | 7 | |a Inorganic chemistry |2 nationallicence | |
| 690 | 7 | |a Organic chemistry |2 nationallicence | |
| 700 | 1 | |a Arıcı |D Cengiz |4 aut | |
| 700 | 1 | |a Ülkü |D Dinçer |4 aut | |
| 700 | 1 | |a Üngören |D S. Hakan |4 aut | |
| 700 | 1 | |a Saçmacı |D Mustafa |4 aut | |
| 700 | 1 | |a Akçamur |D Yunus |4 aut | |
| 773 | 0 | |t Zeitschrift für Kristallographie - Crystalline Materials |d De Gruyter Oldenbourg |g 219/9(2004-09-01), 554-557 |x 2194-4946 |q 219:9<554 |1 2004 |2 219 |o zkri | |
| 856 | 4 | 0 | |u https://doi.org/10.1524/zkri.219.9.554.44037 |q text/html |z Onlinezugriff via DOI |
| 908 | |D 1 |a research article |2 jats | ||
| 950 | |B NATIONALLICENCE |P 856 |E 40 |u https://doi.org/10.1524/zkri.219.9.554.44037 |q text/html |z Onlinezugriff via DOI | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Arıcı |D Cengiz |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Ülkü |D Dinçer |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Üngören |D S. Hakan |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Saçmacı |D Mustafa |4 aut | ||
| 950 | |B NATIONALLICENCE |P 700 |E 1- |a Akçamur |D Yunus |4 aut | ||
| 950 | |B NATIONALLICENCE |P 773 |E 0- |t Zeitschrift für Kristallographie - Crystalline Materials |d De Gruyter Oldenbourg |g 219/9(2004-09-01), 554-557 |x 2194-4946 |q 219:9<554 |1 2004 |2 219 |o zkri | ||
| 900 | 7 | |b CC0 |u http://creativecommons.org/publicdomain/zero/1.0 |2 nationallicence | |
| 898 | |a BK010053 |b XK010053 |c XK010000 | ||
| 949 | |B NATIONALLICENCE |F NATIONALLICENCE |b NL-gruyter | ||