caa a22 4500 378943405 CHVBK 20180305123658.0 cr unu---uuuuu 161128e20040901xx s 000 0 eng 10.1524/zkri.219.9.554.44037 doi (NATIONALLICENCE)gruyter-10.1524/zkri.219.9.554.44037 Structure and characterization of methyl (±)-1-(2-aminophenyl)-2-hydroxy-4-(4-methoxybenzoyl)-5-(4-methoxyphenyl)-3-oxo-2,3-dihydro-1H-pyrrole-2-acetate [Elektronische Daten] [Cengiz Arıcı, Dinçer Ülkü, S. Hakan Üngören, Mustafa Saçmacı, Yunus Akçamur] The stoichiometry of 1 was derived from the results of elemental analysis, IR, 1H, 13C-NMR, UV-Vis and mass spectroscopic techniques. The structure derived from physico-chemical methods is consistent with that of the X-ray diffraction. The compound crystallizes in the triclinic system, space group P1̅, with a = 9.3895(12), b = 11.3759(11), c = 12.8077(14)Å, α = 103.290(3)° β = 98.110(4)°, γ = 105.545(3)°, V = 1252.4(2)Å3, Z = 2. The molecule has a non-planar configuration. The methoxy carbonylmethyl group exhibits an E-configuration. The crystal structure is stabilized by intermolecular C—H O, N—H O and O—H O contacts. © 2004 Oldenbourg Wissenschaftsverlag GmbH Crystallography nationallicence Inorganic chemistry nationallicence Organic chemistry nationallicence Arıcı Cengiz aut Ülkü Dinçer aut Üngören S. Hakan aut Saçmacı Mustafa aut Akçamur Yunus aut Zeitschrift für Kristallographie - Crystalline Materials De Gruyter Oldenbourg 219/9(2004-09-01), 554-557 2194-4946 219:9<554 2004 219 zkri https://doi.org/10.1524/zkri.219.9.554.44037 text/html Onlinezugriff via DOI 1 research article jats NATIONALLICENCE 856 40 https://doi.org/10.1524/zkri.219.9.554.44037 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Arıcı Cengiz aut NATIONALLICENCE 700 1- Ülkü Dinçer aut NATIONALLICENCE 700 1- Üngören S. Hakan aut NATIONALLICENCE 700 1- Saçmacı Mustafa aut NATIONALLICENCE 700 1- Akçamur Yunus aut NATIONALLICENCE 773 0- Zeitschrift für Kristallographie - Crystalline Materials De Gruyter Oldenbourg 219/9(2004-09-01), 554-557 2194-4946 219:9<554 2004 219 zkri CC0 http://creativecommons.org/publicdomain/zero/1.0 nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-gruyter