caa a22 4500 445801182 CHVBK 20180317145141.0 cr unu---uuuuu 170323e20110201xx s 000 0 eng 10.1007/s10337-010-1885-2 doi (NATIONALLICENCE)springer-10.1007/s10337-010-1885-2 Development of an Analytical Method Based on Accelerated Solvent Extraction, Solid-Phase Extraction Clean-Up, then GC-ECD for Analysis of Fourteen Organochlorine Pesticides in Cereal Crops [Elektronische Daten] [Yaping Zhang, Jun Yang, Ronghua Shi, Qingde Su, Yun Gao, Xiaolan Zhu] A method has been developed for analysis of 14 organochlorine pesticide residues in cereals. After accelerated solvent extraction and solid-phase extraction clean-up on graphitized carbon black/primary-secondary amine (GCB/PSA), to reduce co-extraction of interferences, pesticide residues were analyzed by gas chromatography with electron-capture detection. When the method was validated, recoveries were in the range 78-116%, relative standard deviations were in the range 1.1-16.3%, and limits of detection and quantification were from 1.5 to 4.2μgkg−1 and from 4.6 to 12.5μgkg−1, respectively. Springer-Verlag, 2011 Gas chromatography-electron-capture detection nationallicence Accelerated solvent extraction nationallicence Solid-phase extraction nationallicence Cereals nationallicence Organochlorine pesticide residues nationallicence Zhang Yaping Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut Yang Jun Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut Shi Ronghua Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut Su Qingde Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut Gao Yun Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut Zhu Xiaolan Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut Chromatographia Vieweg Verlag 73/3-4(2011-02-01), 385-391 0009-5893 73:3-4<385 2011 73 10337 https://doi.org/10.1007/s10337-010-1885-2 text/html Onlinezugriff via DOI 1 brief-communication jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10337-010-1885-2 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Zhang Yaping Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut NATIONALLICENCE 700 1- Yang Jun Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut NATIONALLICENCE 700 1- Shi Ronghua Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut NATIONALLICENCE 700 1- Su Qingde Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut NATIONALLICENCE 700 1- Gao Yun Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut NATIONALLICENCE 700 1- Zhu Xiaolan Department of Chemistry, University of Science and Technology of China, 230026, Hefei, People's Republic of China aut NATIONALLICENCE 773 0- Chromatographia Vieweg Verlag 73/3-4(2011-02-01), 385-391 0009-5893 73:3-4<385 2011 73 10337 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer