caa a22 4500 445801506 CHVBK 20180317145142.0 cr unu---uuuuu 170323e20110401xx s 000 0 eng 10.1007/s10337-011-1940-7 doi (NATIONALLICENCE)springer-10.1007/s10337-011-1940-7 Simultaneous Determination of 12 Sulfonylurea Herbicides in Drinking Water after SPE by LC-DAD [Elektronische Daten] [Rainer Gallitzendörfer, Thomas Timm, Dagmar Koch, Markus Küsters, Michael Gerhartz] A liquid chromatographic method (LC) with diode array detection (DAD) for the routine screening and quantification of highly applicated polar herbicides in drinking water samples was developed. The investigated herbicides consisted of 12 sulfonylurea herbicides (amidosulfuron, flazasulfuron, foramsulfuron, iodosulfuron-methyl Na, mesosulfuron-methyl, metsulfuron-methyl, nicosulfuron, prosulfuron, thifensulfuron-methyl, triasulfuron and tritosulfuron) together with 6 polar pesticides of relevance (atrazine, desethylatrazine, desisopropylatrazine, chlortoluron, diuron, fluoxypyr). The herbicides were extracted and concentrated by off-line solid-phase extraction and subsequently eluates were analyzed by LC-DAD. Recoveries obtained from fortified water samples at 100ngL−1 were in the range of 84-107% with RSD's <20%. The limit of detection varied from 2 to 16ngL−1. Springer-Verlag, 2011 Column liquid chromatography nationallicence PPL cartridge nationallicence Drinking water nationallicence Phenylurea herbicides nationallicence Pyrimidinylsulfonylurea herbicides nationallicence Triazinylsulfonylurea herbicides nationallicence Gallitzendörfer Rainer Laboratory Department of Food and Environmental Chemistry, Central Institute of the German Federal Armed Forces Medical Service Koblenz, Andernacher Strasse 100, 56070, Koblenz, Germany aut Timm Thomas Laboratory Department of Food and Environmental Chemistry, Central Institute of the German Federal Armed Forces Medical Service Koblenz, Andernacher Strasse 100, 56070, Koblenz, Germany aut Koch Dagmar Laboratory Department of Food and Environmental Chemistry, Central Institute of the German Federal Armed Forces Medical Service Koblenz, Andernacher Strasse 100, 56070, Koblenz, Germany aut Küsters Markus Pharmacy Section, Central Hospital of the German Federal Armed Forces Koblenz, Rübenacher Strasse 170, 56072, Koblenz, Germany aut Gerhartz Michael Laboratory Department of Food and Environmental Chemistry, Central Institute of the German Federal Armed Forces Medical Service Koblenz, Andernacher Strasse 100, 56070, Koblenz, Germany aut Chromatographia Vieweg Verlag 73/7-8(2011-04-01), 813-816 0009-5893 73:7-8<813 2011 73 10337 https://doi.org/10.1007/s10337-011-1940-7 text/html Onlinezugriff via DOI 1 brief-communication jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10337-011-1940-7 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Gallitzendörfer Rainer Laboratory Department of Food and Environmental Chemistry, Central Institute of the German Federal Armed Forces Medical Service Koblenz, Andernacher Strasse 100, 56070, Koblenz, Germany aut NATIONALLICENCE 700 1- Timm Thomas Laboratory Department of Food and Environmental Chemistry, Central Institute of the German Federal Armed Forces Medical Service Koblenz, Andernacher Strasse 100, 56070, Koblenz, Germany aut NATIONALLICENCE 700 1- Koch Dagmar Laboratory Department of Food and Environmental Chemistry, Central Institute of the German Federal Armed Forces Medical Service Koblenz, Andernacher Strasse 100, 56070, Koblenz, Germany aut NATIONALLICENCE 700 1- Küsters Markus Pharmacy Section, Central Hospital of the German Federal Armed Forces Koblenz, Rübenacher Strasse 170, 56072, Koblenz, Germany aut NATIONALLICENCE 700 1- Gerhartz Michael Laboratory Department of Food and Environmental Chemistry, Central Institute of the German Federal Armed Forces Medical Service Koblenz, Andernacher Strasse 100, 56070, Koblenz, Germany aut NATIONALLICENCE 773 0- Chromatographia Vieweg Verlag 73/7-8(2011-04-01), 813-816 0009-5893 73:7-8<813 2011 73 10337 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer