caa a22 4500 445827483 CHVBK 20180317145303.0 cr unu---uuuuu 170323e20110701xx s 000 0 eng 10.1007/s10854-010-0218-4 doi (NATIONALLICENCE)springer-10.1007/s10854-010-0218-4 Synthesis and characterization of pure anatase TiO2 nanoparticles [Elektronische Daten] [B. Shirke, P. Korake, P. Hankare, S. Bamane, K. Garadkar] Pure anatase TiO2 nanoparticles were synthesized by microwave assisted sol-gel method and further characterized by powder X-ray diffraction (XRD), energy dispersive x-ray analysis (EDAX), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and UV-Visible spectrophotometer, SEM images showed that TiO2 nanoparticles were porous structure. The XRD patterns indicated that TiO2 after annealed at 300°C for 3h was mainly pure anatase phase. The crystallite size was in the range of 20-25nm, which is consistent with the results obtained from TEM images. Microwave heating offers several potential advantages over conventional heating for inducing or enhancing chemical reactions. Springer Science+Business Media, LLC, 2010 Shirke B. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut Korake P. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut Hankare P. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut Bamane S. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut Garadkar K. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut Journal of Materials Science: Materials in Electronics Springer US; http://www.springer-ny.com 22/7(2011-07-01), 821-824 0957-4522 22:7<821 2011 22 10854 https://doi.org/10.1007/s10854-010-0218-4 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10854-010-0218-4 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Shirke B. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut NATIONALLICENCE 700 1- Korake P. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut NATIONALLICENCE 700 1- Hankare P. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut NATIONALLICENCE 700 1- Bamane S. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut NATIONALLICENCE 700 1- Garadkar K. Nanomaterials Research Laboratory, Department of Chemistry, Shivaji University, 416004, Kolhapur, India aut NATIONALLICENCE 773 0- Journal of Materials Science: Materials in Electronics Springer US; http://www.springer-ny.com 22/7(2011-07-01), 821-824 0957-4522 22:7<821 2011 22 10854 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer