caa a22 4500 445828188 CHVBK 20180317145305.0 cr unu---uuuuu 170323e20110401xx s 000 0 eng 10.1007/s10854-010-0137-4 doi (NATIONALLICENCE)springer-10.1007/s10854-010-0137-4 Synthesis of deer horn-like and spherical ZnO nanoparticles by microwave decomposition of bis(2-pyridinethiol N -oxide)zinc using factorial and Taguchi experimental designs [Elektronische Daten] [M. Edrissi, R. Norouzbeigi] Deer horn-like and spherical nanoparticles of ZnO have been prepared via microwave heating (MWH) of Bis (2-pyridinethiol N-oxide) Zinc (II) [BPTZ] complex. The product was characterized by XRD, SEM, LLS, BET, FTIR and chemical analysis. The 23 factorial and the Taguchi L 4 designs were used for factors effect estimation and determination of optimum conditions for spherical ZnO nanoparticle synthesis. The three main factors considered were power of microwave, temperature of pyrolysis and time of thermal decomposition. The time of pyrolysis had the most influence on the average particle size and the size distribution of product. The average particle size for the spherical ZnO at optimum conditions was found to be 16nm and the particle range was 16±13nm. Springer Science+Business Media, LLC, 2010 Edrissi M. Faculty of Chemical Engineering (Ex.Ce), Amirkabir University of Technology, Hafez Ave., P. O. Box 15875-4413, Tehran, Iran aut Norouzbeigi R. Faculty of Chemical Engineering (Ex.Ce), Amirkabir University of Technology, Hafez Ave., P. O. Box 15875-4413, Tehran, Iran aut Journal of Materials Science: Materials in Electronics Springer US; http://www.springer-ny.com 22/4(2011-04-01), 328-334 0957-4522 22:4<328 2011 22 10854 https://doi.org/10.1007/s10854-010-0137-4 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10854-010-0137-4 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Edrissi M. Faculty of Chemical Engineering (Ex.Ce), Amirkabir University of Technology, Hafez Ave., P. O. Box 15875-4413, Tehran, Iran aut NATIONALLICENCE 700 1- Norouzbeigi R. Faculty of Chemical Engineering (Ex.Ce), Amirkabir University of Technology, Hafez Ave., P. O. Box 15875-4413, Tehran, Iran aut NATIONALLICENCE 773 0- Journal of Materials Science: Materials in Electronics Springer US; http://www.springer-ny.com 22/4(2011-04-01), 328-334 0957-4522 22:4<328 2011 22 10854 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer