caa a22 4500 445828560 CHVBK 20180317145306.0 cr unu---uuuuu 170323e20110801xx s 000 0 eng 10.1007/s10854-010-0252-2 doi (NATIONALLICENCE)springer-10.1007/s10854-010-0252-2 Preparation and characterization of polyaniline/exfoliated graphite composite via a combination method of in situ polymerization and thermal expansion [Elektronische Daten] [Ji Li, Mei Li, Qian Liu, Hui Da] Polyaniline/exfoliated graphite (PANI/EG) composite was prepared via a combination method of in situ polymerization and thermal expansion and characterized, using scanning electron microscope (SEM), Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD). In the in situ polymerization, PANI/graphite intercalation compounds (GIC) composite was synthesized by GIC and aniline. In the thermal expansion, PANI/EG composite was prepared by PANI/GIC composite. The characterization showed that the morphology of PANI/EG composite was analogous to foam and the surface of PANI/EG composite had many micro-apertures. When PANI/GIC composite was synthesized by 0.80g of GIC and 2.00g of aniline, PANI/GIC composite would be exfoliated to PANI/EG composite at 200°C, which had 75.00mL·g−1 of the expansion volume and 0.01Ω−1cm−1of the conductivity. Springer Science+Business Media, LLC, 2010 Li Ji College of Chemistry and Material Science, Hebei Normal University, 050016, Shijiazhuang, Hebei, China aut Li Mei College of Chemistry and Material Science, Hebei Normal University, 050016, Shijiazhuang, Hebei, China aut Liu Qian College of Chemistry and Material Science, Hebei Normal University, 050016, Shijiazhuang, Hebei, China aut Da Hui College of Chemistry and Material Science, Hebei Normal University, 050016, Shijiazhuang, Hebei, China aut Journal of Materials Science: Materials in Electronics Springer US; http://www.springer-ny.com 22/8(2011-08-01), 1016-1020 0957-4522 22:8<1016 2011 22 10854 https://doi.org/10.1007/s10854-010-0252-2 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10854-010-0252-2 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Li Ji College of Chemistry and Material Science, Hebei Normal University, 050016, Shijiazhuang, Hebei, China aut NATIONALLICENCE 700 1- Li Mei College of Chemistry and Material Science, Hebei Normal University, 050016, Shijiazhuang, Hebei, China aut NATIONALLICENCE 700 1- Liu Qian College of Chemistry and Material Science, Hebei Normal University, 050016, Shijiazhuang, Hebei, China aut NATIONALLICENCE 700 1- Da Hui College of Chemistry and Material Science, Hebei Normal University, 050016, Shijiazhuang, Hebei, China aut NATIONALLICENCE 773 0- Journal of Materials Science: Materials in Electronics Springer US; http://www.springer-ny.com 22/8(2011-08-01), 1016-1020 0957-4522 22:8<1016 2011 22 10854 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer