caa a22 4500 445879807 CHVBK 20180317145539.0 cr unu---uuuuu 170323e20110201xx s 000 0 eng 10.1007/s00604-010-0473-3 doi (NATIONALLICENCE)springer-10.1007/s00604-010-0473-3 Microwave assisted extraction for mercury speciation analysis [Elektronische Daten] [Laura Reyes, Jorge Mar, Aracely Hernández-Ramírez, Juan Peralta-Hernández, Juan Barbosa, H. Kingston] The application of microwave-assisted extraction (MAE) to the work-up of environmental and biological samples in the study of mercury speciation analysis has increased in recent years and is now increasingly accepted as a standard approach. The review provides a brief theoretical background of microwave heating and the basic principles of microwave energy used for extraction. The advantages and disadvantages of (a) MAE techniques, (b) the influence of the main parameters affecting the extraction, (c) statistical optimization approaches, and (d) strategies for method validation also are highlighted. Recent applications of MAE to mercury species analyses in biological samples, soils, sediments, and crude oil samples are surveyed and critically reviewed. In addition, comparisons of its use with other well-established extraction procedures are discussed. Figure Microwave-assisted extraction has become a very useful sample preparation techniques in the study of mercury speciation in environmental and biological samples Springer-Verlag, 2010 Microwave-assisted extraction (MAE) nationallicence Sample preparation nationallicence Speciation analysis nationallicence Mercury nationallicence Mercury species nationallicence Method validation nationallicence Reyes Laura Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut Mar Jorge Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut Hernández-Ramírez Aracely Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut Peralta-Hernández Juan Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut Barbosa Juan Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut Kingston H. Department of Chemistry and Biochemistry, Duquesne University, 15282, Pittsburgh, PA, USA aut Microchimica Acta Springer Vienna 172/1-2(2011-02-01), 3-14 0026-3672 172:1-2<3 2011 172 604 https://doi.org/10.1007/s00604-010-0473-3 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s00604-010-0473-3 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Reyes Laura Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut NATIONALLICENCE 700 1- Mar Jorge Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut NATIONALLICENCE 700 1- Hernández-Ramírez Aracely Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut NATIONALLICENCE 700 1- Peralta-Hernández Juan Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut NATIONALLICENCE 700 1- Barbosa Juan Facultad de Ciencias Químicas, Universidad Autónoma de Nuevo León, Cd. Universitaria, 66400, San Nicolás de los Garza, NL, México aut NATIONALLICENCE 700 1- Kingston H. Department of Chemistry and Biochemistry, Duquesne University, 15282, Pittsburgh, PA, USA aut NATIONALLICENCE 773 0- Microchimica Acta Springer Vienna 172/1-2(2011-02-01), 3-14 0026-3672 172:1-2<3 2011 172 604 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer