caa a22 4500 463157567 CHVBK 20180406164738.0 cr unu---uuuuu 170326e20070301xx s 000 0 eng 10.1007/s00217-006-0350-9 doi (NATIONALLICENCE)springer-10.1007/s00217-006-0350-9 Determination of bisphenol A in canned fish by sol-gel immunoaffinity chromatography, HPLC and fluorescence detection [Elektronische Daten] [Dagmar Podlipna, Margit Cichna-Markl] The paper presents a highly selective analysis method for the determination of bisphenol A (BPA) in canned fish. The procedure consists of sample clean-up by sol-gel immunoaffinity chromatography followed by high performance liquid chromatography and fluorescence detection. BPA concentrations were determined in nineteen tuna, sardine and mackerel cans by analysing the solid and the liquid parts of the contents separately. In different tested matrices limits of detection (S/N=3) ranged from 0.2ng/g (sardines) to 1.8ng/ml (oil) and limits of quantification (S/N=6) from 0.4ng/g to 3.8ng/ml, respectively. In the solid part (fish) very low BPA levels (2-4ng/g) were found in mackerels, the highest level (59ng/g) in tuna. In oil significantly higher BPA concentrations were found than in brine. In all samples BPA concentrations were significantly lower than the Specific Migration Level of 0.6mg/kg for BPA migration into food established by the EU Commission in 2004. Springer-Verlag, 2006 Bisphenol A nationallicence Fish nationallicence Fish cans nationallicence Migration nationallicence Immunoaffinity chromatography nationallicence Sol-gel nationallicence Podlipna Dagmar Department of Analytical and Food Chemistry, University of Vienna, Währinger Straße 38, A-1090, Vienna, Austria aut Cichna-Markl Margit Department of Analytical and Food Chemistry, University of Vienna, Währinger Straße 38, A-1090, Vienna, Austria aut European Food Research and Technology Springer-Verlag 224/5(2007-03-01), 629-634 1438-2377 224:5<629 2007 224 217 https://doi.org/10.1007/s00217-006-0350-9 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s00217-006-0350-9 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Podlipna Dagmar Department of Analytical and Food Chemistry, University of Vienna, Währinger Straße 38, A-1090, Vienna, Austria aut NATIONALLICENCE 700 1- Cichna-Markl Margit Department of Analytical and Food Chemistry, University of Vienna, Währinger Straße 38, A-1090, Vienna, Austria aut NATIONALLICENCE 773 0- European Food Research and Technology Springer-Verlag 224/5(2007-03-01), 629-634 1438-2377 224:5<629 2007 224 217 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer