caa a22 4500 463185005 CHVBK 20180406164850.0 cr unu---uuuuu 170326e20070201xx s 000 0 eng 10.1007/s10870-006-9155-8 doi (NATIONALLICENCE)springer-10.1007/s10870-006-9155-8 Single crystals of calcium and strontium phenylphosphonate grown via hydrothermal crystallization [Elektronische Daten] [John Stone, Mark Smith, Hans-Conrad Loye] : Single crystals of Ca(HO3PC6H5)2 (1) and Sr(HO3PC6H5)2 (2) have been obtained via the crystallization of their respective amorphous powders. The amorphous compounds were synthesized by traditional solution routes and were subsequently crystallized at 160°C in a Teflon-lined autoclave containing 1-3mL distilled water. The resultant single crystals were physically isolated and their structures determined by single crystal X-ray diffraction. The two compounds are isostructural and crystallize in space group C2/c with lattice parameters of a=31.267(3)Å, b=5.6185(6)Å, c=7.7202(8)Å, β=101.924(2)°; and a=31.514(4)Å, b=5.8098(8)Å, c=7.8218(10)Å, β=102.063(3)° for the calcium and strontium phenylphosphonate, respectively. Springer Science+Business Media, LLC, 2006 metal phosphonate nationallicence layered structure nationallicence crystal structure nationallicence hydrothermal crystallization nationallicence Stone John Department of Chemistry and Biochemistry, University of South Carolina, 631 Sumter St., 29208, Columbia, SC, US aut Smith Mark Department of Chemistry and Biochemistry, University of South Carolina, 631 Sumter St., 29208, Columbia, SC, US aut Loye Hans-Conrad Department of Chemistry and Biochemistry, University of South Carolina, 631 Sumter St., 29208, Columbia, SC, US aut Journal of Chemical Crystallography Springer US; http://www.springer-ny.com 37/2(2007-02-01), 103-108 1074-1542 37:2<103 2007 37 10870 https://doi.org/10.1007/s10870-006-9155-8 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10870-006-9155-8 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Stone John Department of Chemistry and Biochemistry, University of South Carolina, 631 Sumter St., 29208, Columbia, SC, US aut NATIONALLICENCE 700 1- Smith Mark Department of Chemistry and Biochemistry, University of South Carolina, 631 Sumter St., 29208, Columbia, SC, US aut NATIONALLICENCE 700 1- Loye Hans-Conrad Department of Chemistry and Biochemistry, University of South Carolina, 631 Sumter St., 29208, Columbia, SC, US aut NATIONALLICENCE 773 0- Journal of Chemical Crystallography Springer US; http://www.springer-ny.com 37/2(2007-02-01), 103-108 1074-1542 37:2<103 2007 37 10870 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer