caa a22 4500 463187997 CHVBK 20180406164859.0 cr unu---uuuuu 170326e20070401xx s 000 0 eng 10.1007/s10973-006-8075-3 doi (NATIONALLICENCE)springer-10.1007/s10973-006-8075-3 Synthesisand characterization of alumina- and zirconia-based powders obtained by theultrasonic spray pyrolysis [Elektronische Daten] [W. Kucza, J. Obłąkowski, R. Gajerski, S. Łabuś, M. Danielewski, A. Małecki, J. Morgiel, A. Michalski] The ultrasonic spray pyrolysis (USP) technique was used for synthesis of alumina- and zirconia-based powders. The starting agents were aqueous solutions, atomized by the ultrasonic spray generator and pyrolized in the furnace under the open-air conditions. The powders prepared by USP were in the form of solid and hollow aggregates (spheres) consisted of nanosize amorphous grains as determined by the microscopy and the X-ray diffraction techniques. The alumina-based powders were consolidated by the pulse plasma sintering resulting in single-phase materials. Different behavior of solid and hollow particles during the isostatic sintering is found; a higher degree of deformation of spheres is observed in the second case. Springer-Verlag, 2007 alumina nationallicence plasma sintering nationallicence SEM nationallicence spray pyrolysis nationallicence TEM nationallicence zirconia nationallicence Kucza W. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut Obłąkowski J. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut Gajerski R. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut Łabuś S. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut Danielewski M. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut Małecki A. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut Morgiel J. Institute of Metallurgy and Materials Sciences, Polish Academy of Sciences, Reymonta 25, 30-059, Cracow, Poland aut Michalski A. Faculty of Materials Science and Engineering, Warsaw University of Technology, Wołoska 141, 02-507, Warsaw, Poland aut Journal of Thermal Analysis and Calorimetry Kluwer Academic Publishers 88/1(2007-04-01), 65-69 1388-6150 88:1<65 2007 88 10973 https://doi.org/10.1007/s10973-006-8075-3 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10973-006-8075-3 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Kucza W. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut NATIONALLICENCE 700 1- Obłąkowski J. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut NATIONALLICENCE 700 1- Gajerski R. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut NATIONALLICENCE 700 1- Łabuś S. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut NATIONALLICENCE 700 1- Danielewski M. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut NATIONALLICENCE 700 1- Małecki A. Faculty of Materials Science and Ceramics, AGH University of Science and Technology, Al. Mickiewicza 30, 30-059, Cracow, Poland aut NATIONALLICENCE 700 1- Morgiel J. Institute of Metallurgy and Materials Sciences, Polish Academy of Sciences, Reymonta 25, 30-059, Cracow, Poland aut NATIONALLICENCE 700 1- Michalski A. Faculty of Materials Science and Engineering, Warsaw University of Technology, Wołoska 141, 02-507, Warsaw, Poland aut NATIONALLICENCE 773 0- Journal of Thermal Analysis and Calorimetry Kluwer Academic Publishers 88/1(2007-04-01), 65-69 1388-6150 88:1<65 2007 88 10973 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer