caa a22 4500 463189760 CHVBK 20180406164905.0 cr unu---uuuuu 170326e20071201xx s 000 0 eng 10.1007/s10973-005-7060-6 doi (NATIONALLICENCE)springer-10.1007/s10973-005-7060-6 Solid-state compounds of 2-chlorobenzylidenepyruvate with some bivalent metal ions [Elektronische Daten] Synthesis, characterization and thermal behaviour [G. Bannach, A. Siqueira, E. Ionashiro, E. Rodrigues, M. Ionashiro] Solid-state M-2-Cl-BP, where M stands for Mn, Fe, Co, Ni, Cu, Zn and Pb and 2-Cl-BP is 2-chlorobenzylidenepyruvate, have been synthesized. Thermogravimetry and derivative thermogravimetry (TG/DTG), simultaneous thermogravimetry and differential thermal analysis (TG-DTA), X-ray powder diffractometry, infrared spectroscopy, elemental analysis, and complexometry were used to characterize and to study the thermal behaviour of these compounds. The results led to information about the composition, dehydration, thermal stability and thermal decomposition of the isolated compounds. Springer Science+Business Media, LLC., 2007 bivalent metals nationallicence 2-chlorobenzylidenepyruvate nationallicence coordination sites nationallicence thermal behaviour nationallicence Bannach G. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut Siqueira A. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut Ionashiro E. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut Rodrigues E. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut Ionashiro M. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut Journal of Thermal Analysis and Calorimetry Springer US; http://www.springer-ny.com 90/3(2007-12-01), 873-879 1388-6150 90:3<873 2007 90 10973 https://doi.org/10.1007/s10973-005-7060-6 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10973-005-7060-6 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Bannach G. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut NATIONALLICENCE 700 1- Siqueira A. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut NATIONALLICENCE 700 1- Ionashiro E. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut NATIONALLICENCE 700 1- Rodrigues E. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut NATIONALLICENCE 700 1- Ionashiro M. Instituto de Química, UNESP, CP 355, CEP 14801-970, Araraquara, SP, Brazil aut NATIONALLICENCE 773 0- Journal of Thermal Analysis and Calorimetry Springer US; http://www.springer-ny.com 90/3(2007-12-01), 873-879 1388-6150 90:3<873 2007 90 10973 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer