caa a22 4500 463189884 CHVBK 20180406164905.0 cr unu---uuuuu 170326e20071201xx s 000 0 eng 10.1007/s10973-006-8248-0 doi (NATIONALLICENCE)springer-10.1007/s10973-006-8248-0 XRD, TEM and thermal analysis of Fe doped boehmite nanofibres and nanosheets [Elektronische Daten] [Y. Zhao, R. Frost, W. Martens, H. Zhu] Iron doped boehmite nanofibres with varying iron content have been prepared at low temperatures using a hydrothermal treatment in the presence of poly(ethylene oxide) surfactant. The resultant nanofibres were characterized by X-ray diffraction (XRD), and transmission electron microscopy (TEM). TEM images showed the resulting nanostructures are predominantly nanofibres when Fe doping is no more than 5%; in contrast nanosheets were formed if Fe doping was above 5%. For the 10% Fe doped boehmite, a mixed morphology of nanofibres and nanosheets were obtained. Nanotubes instead of nanofibres were observed in samples with 20% added iron. The Fe doped boehmite and the subsequent nanofibres/nanotubes were analysed by thermogravimetric and differential thermogravimetric methods. Boehmite nanofibres decompose at higher temperatures than non-hydrothermally treated boehmite and nano-sheets decompose at lower temperatures than the nanofibres. Springer Science+Business Media LLC, 2007 acicular nationallicence boehmite nationallicence nanofibre nationallicence nanosheets nationallicence nanotube nationallicence Zhao Y. Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, GPO Box 2434, 4001, Brisbane, Queensland, Australia aut Frost R. Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, GPO Box 2434, 4001, Brisbane, Queensland, Australia aut Martens W. Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, GPO Box 2434, 4001, Brisbane, Queensland, Australia aut Zhu H. Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, GPO Box 2434, 4001, Brisbane, Queensland, Australia aut Journal of Thermal Analysis and Calorimetry Springer US; http://www.springer-ny.com 90/3(2007-12-01), 755-760 1388-6150 90:3<755 2007 90 10973 https://doi.org/10.1007/s10973-006-8248-0 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10973-006-8248-0 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Zhao Y. Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, GPO Box 2434, 4001, Brisbane, Queensland, Australia aut NATIONALLICENCE 700 1- Frost R. Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, GPO Box 2434, 4001, Brisbane, Queensland, Australia aut NATIONALLICENCE 700 1- Martens W. Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, GPO Box 2434, 4001, Brisbane, Queensland, Australia aut NATIONALLICENCE 700 1- Zhu H. Inorganic Materials Research Program, School of Physical and Chemical Sciences, Queensland University of Technology, GPO Box 2434, 4001, Brisbane, Queensland, Australia aut NATIONALLICENCE 773 0- Journal of Thermal Analysis and Calorimetry Springer US; http://www.springer-ny.com 90/3(2007-12-01), 755-760 1388-6150 90:3<755 2007 90 10973 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer