caa a22 4500 463191919 CHVBK 20180406164911.0 cr unu---uuuuu 170326e20070801xx s 000 0 eng 10.1007/s10973-006-7532-3 doi (NATIONALLICENCE)springer-10.1007/s10973-006-7532-3 Non-isothermal kinetic study on the decomposition of Zn acetate-based Sol-gel precursor [Elektronische Daten] Part 1. Application of the isoconversional methods [V. Muşat, P. Budrugeac, R. Monteiro, E. Fortunato, E. Segal] The isoconversional methods (Friedman (FR), Flynn-Wall-Ozawa (FWO) and Kissinger-Akahira-Sunose (KAS)) were applied for evaluating the dependencies of the activation energy (E) on the mass loss (Δm) corresponding to the non-isothermal decomposition of two Zn acetate-based gel precursors for ZnO thin films whose preparation differs by the drying temperature of the liquid sol-precursor (125°C for sample A, and 150°C for sample B). Although both investigated samples exhibit similar decomposition steps, strong differences between E vs. Δm curves as well as among the characteristic parameters of the decomposition steps, directly evaluated from TG, DTG and DTA curves, were put in evidence. Springer Science+Business Media LLC, 2007 isoconversional kinetic methods nationallicence sol-gel nationallicence TG-DTG-DTA nationallicence thermal decomposition nationallicence Zn acetate-based precursor nationallicence Muşat V. Department of Metals and Materials Science, ‘Dunărea de Jos' University of Galati, 111 Domneasca, 800201, Galati, Romania aut Budrugeac P. INCDIE-ICPE-CA-National Institute for Research and Development in Electrical Engineering, 313 Splaiul Unirii, 030138, Bucharest, Romania aut Monteiro R. Department of Materials Science, CENIMAT, Faculty of Sciences and Technology, New University of Lisbon, Quinta da Torre, 2829-516, Caparica, Portugal aut Fortunato E. Department of Materials Science, CENIMAT, Faculty of Sciences and Technology, New University of Lisbon, Quinta da Torre, 2829-516, Caparica, Portugal aut Segal E. Department of Physical Chemistry, University of Bucharest, 4-12 Bd. Elisabeta, 7034, Bucharest, Romania aut Journal of Thermal Analysis and Calorimetry Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 89/2(2007-08-01), 505-509 1388-6150 89:2<505 2007 89 10973 https://doi.org/10.1007/s10973-006-7532-3 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10973-006-7532-3 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Muşat V. Department of Metals and Materials Science, ‘Dunărea de Jos' University of Galati, 111 Domneasca, 800201, Galati, Romania aut NATIONALLICENCE 700 1- Budrugeac P. INCDIE-ICPE-CA-National Institute for Research and Development in Electrical Engineering, 313 Splaiul Unirii, 030138, Bucharest, Romania aut NATIONALLICENCE 700 1- Monteiro R. Department of Materials Science, CENIMAT, Faculty of Sciences and Technology, New University of Lisbon, Quinta da Torre, 2829-516, Caparica, Portugal aut NATIONALLICENCE 700 1- Fortunato E. Department of Materials Science, CENIMAT, Faculty of Sciences and Technology, New University of Lisbon, Quinta da Torre, 2829-516, Caparica, Portugal aut NATIONALLICENCE 700 1- Segal E. Department of Physical Chemistry, University of Bucharest, 4-12 Bd. Elisabeta, 7034, Bucharest, Romania aut NATIONALLICENCE 773 0- Journal of Thermal Analysis and Calorimetry Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 89/2(2007-08-01), 505-509 1388-6150 89:2<505 2007 89 10973 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer