caa a22 4500 463192028 CHVBK 20180406164912.0 cr unu---uuuuu 170326e20070801xx s 000 0 eng 10.1007/s10973-006-7510-9 doi (NATIONALLICENCE)springer-10.1007/s10973-006-7510-9 Low-temperature heat capacity and thermodynamic properties of crystalline lead formate [Elektronische Daten] [J. Zhang, Y. Liu, Z. Zhang, X. Lv, L. Sun, F. Xu, Z. Tan, T. Zhang, Y. Sawada] As one 3-D coordination polymer, lead formate was synthesized; calorimetric study and thermal analysis for this compound were performed. The low-temperature heat capacity of lead formate was measured by a precise automated adiabatic calorimeter over the temperature range from 80 to 380 K. No thermal anomaly or phase transition was observed in this temperature range. A four-step sequential thermal decomposition mechanism for the lead formate was found through the DSC and TG-DTG techniques at the temperature range from 500 to 635 K. Springer Science+Business Media LLC, 2007 adiabatic calorimetry nationallicence coordination polymers nationallicence DSC nationallicence heat capacity nationallicence lead formate nationallicence phase transition nationallicence TG-DTG nationallicence Zhang J. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut Liu Y. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut Zhang Z. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut Lv X. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut Sun L. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut Xu F. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut Tan Z. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut Zhang T. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut Sawada Y. Department of Nanochemistry, Faculty of Engineering, Tokyo Polytechnic University, 1583 Iiyama, Atsugi, 243-0297, Kanagawa, Japan aut Journal of Thermal Analysis and Calorimetry Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 89/2(2007-08-01), 643-647 1388-6150 89:2<643 2007 89 10973 https://doi.org/10.1007/s10973-006-7510-9 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10973-006-7510-9 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Zhang J. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut NATIONALLICENCE 700 1- Liu Y. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut NATIONALLICENCE 700 1- Zhang Z. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut NATIONALLICENCE 700 1- Lv X. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut NATIONALLICENCE 700 1- Sun L. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut NATIONALLICENCE 700 1- Xu F. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut NATIONALLICENCE 700 1- Tan Z. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut NATIONALLICENCE 700 1- Zhang T. Materials and Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116023, Dalian, P.R. China aut NATIONALLICENCE 700 1- Sawada Y. Department of Nanochemistry, Faculty of Engineering, Tokyo Polytechnic University, 1583 Iiyama, Atsugi, 243-0297, Kanagawa, Japan aut NATIONALLICENCE 773 0- Journal of Thermal Analysis and Calorimetry Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 89/2(2007-08-01), 643-647 1388-6150 89:2<643 2007 89 10973 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer