caa a22 4500 463192729 CHVBK 20180406164913.0 cr unu---uuuuu 170326e20070301xx s 000 0 eng 10.1007/s10973-006-7760-6 doi (NATIONALLICENCE)springer-10.1007/s10973-006-7760-6 Synthesisand characterization of Pb1-xLaxTiO3nanocrystalline powders [Elektronische Daten] [A. Mesquita, M. Bernardi, L. Maia, V. Mastelaro] Pb1-xLaxTiO3 (PLT) nanocrystalline powders were obtained by polymeric precursor method. The samples were analyzed by differential scanning calorimetry (DSC) and thermogravimetry (TG) techniques to characterize properly the distinct thermal events occurring during synthesis. The X-ray diffraction patterns show a tetragonal structure for the samples with x=0.10 and 0.15. An increase of the lanthanum concentration to x=0.20 led to a highly symmetric structure, cubic on average. The powders obtained at the end of the synthesis had an average particle size of 30 to 70 nm. Springer-Verlag, 2007 nanocrystalline powders nationallicence Pb1-xLaxTiO3 nationallicence polymeric precursors nationallicence Mesquita A. Instituto de Física de São Carlos, Universidade de São Paulo, São Carlos, SP, Brazil aut Bernardi M. Instituto de Física de São Carlos, Universidade de São Paulo, São Carlos, SP, Brazil aut Maia L. Instituto de Física de São Carlos, Universidade de São Paulo, São Carlos, SP, Brazil aut Mastelaro V. Instituto de Física de São Carlos, Universidade de São Paulo, São Carlos, SP, Brazil aut Journal of Thermal Analysis and Calorimetry Kluwer Academic Publishers 87/3(2007-03-01), 747-751 1388-6150 87:3<747 2007 87 10973 https://doi.org/10.1007/s10973-006-7760-6 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10973-006-7760-6 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Mesquita A. Instituto de Física de São Carlos, Universidade de São Paulo, São Carlos, SP, Brazil aut NATIONALLICENCE 700 1- Bernardi M. Instituto de Física de São Carlos, Universidade de São Paulo, São Carlos, SP, Brazil aut NATIONALLICENCE 700 1- Maia L. Instituto de Física de São Carlos, Universidade de São Paulo, São Carlos, SP, Brazil aut NATIONALLICENCE 700 1- Mastelaro V. Instituto de Física de São Carlos, Universidade de São Paulo, São Carlos, SP, Brazil aut NATIONALLICENCE 773 0- Journal of Thermal Analysis and Calorimetry Kluwer Academic Publishers 87/3(2007-03-01), 747-751 1388-6150 87:3<747 2007 87 10973 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer