caa a22 4500 463212363 CHVBK 20180405153145.0 cr unu---uuuuu 170326e20071001xx s 000 0 eng 10.1007/s00339-007-4073-y doi (NATIONALLICENCE)springer-10.1007/s00339-007-4073-y Synthesis of high-purity α- and β-PbO and possible applications to synthesis and processing of other lead oxide materials [Elektronische Daten] [D.L. Perry, T.J. Wilkinson] Litharge, the red tetragonal form of lead oxide α-PbO and massicot, the yellow orthorhombic form β-PbO, are synthesized from lead(II) salts in aqueous media at elevated temperatures. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used to characterize the size, morphology, and crystallographic structural forms of the products. The role of impurities in the experimental synthesis of the materials and microstructural variations in the final products are described. The implications of these observations regarding the synthesis of different conducting lead oxides and other related materials are discussed. Springer-Verlag, 2007 Perry D.L. Lawrence Berkeley National Laboratory, MS 70A1150, Sensors Group, University of California, 94720, Berkeley, CA, USA aut Wilkinson T.J. Lawrence Berkeley National Laboratory, MS 70A1150, Sensors Group, University of California, 94720, Berkeley, CA, USA aut Applied Physics A Springer-Verlag 89/1(2007-10-01), 77-80 0947-8396 89:1<77 2007 89 339 https://doi.org/10.1007/s00339-007-4073-y text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s00339-007-4073-y text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Perry D.L. Lawrence Berkeley National Laboratory, MS 70A1150, Sensors Group, University of California, 94720, Berkeley, CA, USA aut NATIONALLICENCE 700 1- Wilkinson T.J. Lawrence Berkeley National Laboratory, MS 70A1150, Sensors Group, University of California, 94720, Berkeley, CA, USA aut NATIONALLICENCE 773 0- Applied Physics A Springer-Verlag 89/1(2007-10-01), 77-80 0947-8396 89:1<77 2007 89 339 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer