caa a22 4500 463212754 CHVBK 20180405153146.0 cr unu---uuuuu 170326e20071101xx s 000 0 eng 10.1007/s00339-007-4172-9 doi (NATIONALLICENCE)springer-10.1007/s00339-007-4172-9 Regular hexagonal MoS2 microflakes grown from MoO3 precursor [Elektronische Daten] [G.M. Cai, J.K. Jian, X.L. Chen, M. Lei, W.Y. Wang] Regular hexagonal MoS2 microflakes with high yield were grown from MoO3 precursor by a sulfurization process using S powders as sulfuration reducer. The precursors, long and smooth MoO3 microbelts, were synthesized through a direct oxidation reaction of Mo plates in air. X-ray powder diffraction and scanning electron microscopy revealed that the sulfurized products were hexagonal MoS2 with regular hexagonal flake-like morphology. The results of transmission electron microscopy examinations demonstrated that the microflakes were single crystalline MoS2. Elemental analysis by EDAX and XPS showed that the microflakes consist of Mo and S with the atomic ratio near to 0.5. Factors influencing the formation of the product were systematically studied. Springer-Verlag, 2007 Cai G.M. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut Jian J.K. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut Chen X.L. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut Lei M. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut Wang W.Y. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut Applied Physics A Springer-Verlag 89/3(2007-11-01), 783-788 0947-8396 89:3<783 2007 89 339 https://doi.org/10.1007/s00339-007-4172-9 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s00339-007-4172-9 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Cai G.M. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut NATIONALLICENCE 700 1- Jian J.K. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut NATIONALLICENCE 700 1- Chen X.L. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut NATIONALLICENCE 700 1- Lei M. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut NATIONALLICENCE 700 1- Wang W.Y. Beijing National Laboratory for Condensed Matter Physics, Institute of Physics, Chinese Academy of Sciences, P.O. Box 603, 100080, Beijing, P.R. China aut NATIONALLICENCE 773 0- Applied Physics A Springer-Verlag 89/3(2007-11-01), 783-788 0947-8396 89:3<783 2007 89 339 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer