caa a22 4500 463214986 CHVBK 20180405153153.0 cr unu---uuuuu 170326e20070401xx s 000 0 eng 10.1007/s00339-006-3860-1 doi (NATIONALLICENCE)springer-10.1007/s00339-006-3860-1 Synthesis and structural characterization of the antiferroelectric lead zirconate nanotubes by pulsed laser deposition [Elektronische Daten] [S. Singh, S.B. Krupanidhi] For the first time, a pulsed laser ablation deposition (PLD) method has been employed for the synthesis of antiferroelectric lead zirconate, PbZrO3, (PZ) nanotubes within the pores of anodic aluminum oxide (AAO) templates. The structure and morphology of fabricated PZ nanotubes were characterized by number of techniques, including scanning electron microscope (SEM), X-ray diffraction (XRD) and transmission electron microscope (TEM)analysis. After postannealing at 650°C, the PZ nanotubes exhibited a polycrystalline microstructure, and X-ray diffraction studies revealed that they are of an orthorhombic distorted perovskite crystal structure. TEM analysis confirmed that the obtained PZ nanotubes are composed of nanoparticles in the range of 3-7nm and the thickness of the wall of the nanotubes is around 10nm. Springer-Verlag, 2007 Singh S. Materials Research Centre, Indian Institute of Science, 560012, Bangalore, India aut Krupanidhi S.B. Materials Research Centre, Indian Institute of Science, 560012, Bangalore, India aut Applied Physics A Springer-Verlag 87/1(2007-04-01), 27-30 0947-8396 87:1<27 2007 87 339 https://doi.org/10.1007/s00339-006-3860-1 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s00339-006-3860-1 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Singh S. Materials Research Centre, Indian Institute of Science, 560012, Bangalore, India aut NATIONALLICENCE 700 1- Krupanidhi S.B. Materials Research Centre, Indian Institute of Science, 560012, Bangalore, India aut NATIONALLICENCE 773 0- Applied Physics A Springer-Verlag 87/1(2007-04-01), 27-30 0947-8396 87:1<27 2007 87 339 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer