caa a22 4500 463217209 CHVBK 20180405153200.0 cr unu---uuuuu 170326e20071101xx s 000 0 eng 10.1007/s00269-007-0180-8 doi (NATIONALLICENCE)springer-10.1007/s00269-007-0180-8 Neutron diffraction study of aluminous hydroxide δ-AlOOD [Elektronische Daten] [C. Vanpeteghem, A. Sano, K. Komatsu, E. Ohtani, A. Suzuki] We have determined the position of deuterium atoms in δ-AlOOD by neutron powder diffraction at ambient pressure. As previously reported by theoretical and experimental studies, the deuterium atoms are located in the tunnel formed by the chains of AlO6 octahedra. The data are best fit with the P21 nm structure, producing bond lengths of D-O1 of 1.552(2)Å, O2-D of 1.020(2)Å and O1-O2 of 2.571(2). This study confirms that the hydrogen bond is asymmetric at ambient conditions in agreement with recent single-crystal synchrotron study for δ-AlOOH. Springer-Verlag, 2007 Neutron diffraction nationallicence Hydrogen bond nationallicence Crystal structure nationallicence Vanpeteghem C. School of Chemistry and Biochemistry, Georgia Institute of Technology, 30332, Atlanta, GA, USA aut Sano A. Institute of Mineralogy, Petrology and Economic Geology, Graduate School of Science, Tohoku University, Aramaki Aoba, Aoba, 980-8578, Sendai, Japan aut Komatsu K. Centre for Science at Extreme Conditions, The University of Edinburgh, Mayfield Road, EH9 3JZ, Edinburgh, UK aut Ohtani E. Institute of Mineralogy, Petrology and Economic Geology, Graduate School of Science, Tohoku University, Aramaki Aoba, Aoba, 980-8578, Sendai, Japan aut Suzuki A. Institute of Mineralogy, Petrology and Economic Geology, Graduate School of Science, Tohoku University, Aramaki Aoba, Aoba, 980-8578, Sendai, Japan aut Physics and Chemistry of Minerals Springer-Verlag 34/9(2007-11-01), 657-661 0342-1791 34:9<657 2007 34 269 https://doi.org/10.1007/s00269-007-0180-8 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s00269-007-0180-8 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Vanpeteghem C. School of Chemistry and Biochemistry, Georgia Institute of Technology, 30332, Atlanta, GA, USA aut NATIONALLICENCE 700 1- Sano A. Institute of Mineralogy, Petrology and Economic Geology, Graduate School of Science, Tohoku University, Aramaki Aoba, Aoba, 980-8578, Sendai, Japan aut NATIONALLICENCE 700 1- Komatsu K. Centre for Science at Extreme Conditions, The University of Edinburgh, Mayfield Road, EH9 3JZ, Edinburgh, UK aut NATIONALLICENCE 700 1- Ohtani E. Institute of Mineralogy, Petrology and Economic Geology, Graduate School of Science, Tohoku University, Aramaki Aoba, Aoba, 980-8578, Sendai, Japan aut NATIONALLICENCE 700 1- Suzuki A. Institute of Mineralogy, Petrology and Economic Geology, Graduate School of Science, Tohoku University, Aramaki Aoba, Aoba, 980-8578, Sendai, Japan aut NATIONALLICENCE 773 0- Physics and Chemistry of Minerals Springer-Verlag 34/9(2007-11-01), 657-661 0342-1791 34:9<657 2007 34 269 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer