caa a22 4500 463218930 CHVBK 20180405153206.0 cr unu---uuuuu 170326e20070901xx s 000 0 eng 10.1134/S1061934807090109 doi (NATIONALLICENCE)springer-10.1134/S1061934807090109 Simultaneous determination of residual polychlorinated biphenyls and organochlorine pesticides in fish and fish products by gas-liquid chromatography [Elektronische Daten] [E. Barkatina, I. Zastenskaya, O. Shulyakovskaya, A. Pertsovskii, N. Bunevich, T. Fedorova] A procedure is developed for the simultaneous determination of polychlorinated biphenyls and organochlorine pesticides in fish and fish products by gas-liquid chromatography with an electron capture detector on a capillary column DB-1701 (30 m × 0.25 mm × 0.25 μm) under temperature-programming conditions. The detection limit is 0.06 μg/kg of the test sample. Polychlorinated biphenyls and organochlorine pesticides were extracted from the samples using a hexane-acetone mixture (1 : 1). Lipids were removed by treatment with H2SO4. Eighteen samples were analyzed; the concentrations of pollutants were found to be below the prescribed values. Pleiades Publishing, Ltd., 2007 Barkatina E. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut Zastenskaya I. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut Shulyakovskaya O. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut Pertsovskii A. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut Bunevich N. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut Fedorova T. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut Journal of Analytical Chemistry Nauka/Interperiodica 62/9(2007-09-01), 868-871 1061-9348 62:9<868 2007 62 10809 https://doi.org/10.1134/S1061934807090109 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1134/S1061934807090109 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Barkatina E. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut NATIONALLICENCE 700 1- Zastenskaya I. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut NATIONALLICENCE 700 1- Shulyakovskaya O. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut NATIONALLICENCE 700 1- Pertsovskii A. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut NATIONALLICENCE 700 1- Bunevich N. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut NATIONALLICENCE 700 1- Fedorova T. GU Republican Research and Applied Center for Hygiene of the Ministry of Public Health of the Republic of Belarus, ul. Akademicheskaya 8, 220012, Minsk, Belarus aut NATIONALLICENCE 773 0- Journal of Analytical Chemistry Nauka/Interperiodica 62/9(2007-09-01), 868-871 1061-9348 62:9<868 2007 62 10809 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer