caa a22 4500 463220978 CHVBK 20180405153212.0 cr unu---uuuuu 170326e20070101xx s 000 0 eng 10.1007/s10853-006-1055-y doi (NATIONALLICENCE)springer-10.1007/s10853-006-1055-y Preparation of Pb(Zr,Ti)O3-Pb(Mg1/3Nb2/3)O3 piezoelectric ceramics by dry-dry method [Elektronische Daten] [Yugong Wu, Bin Wang, Zhibo Cong, Bu Wang] Ternary perovskite ceramics of Pb[(Zr0.5Ti0.5)0.8−x (Mg1/3Nb2/3)0.2+x]0.98Nb0.02O3.01 (PZTMN, x=−0.075, −0.05, −0.025, 0, 0.025, 0.05, and 0.075 ), are synthesized via dry-dry method. B-site precursors of PZTMN ([(Zr0.5Ti0.5)0.8−x (Mg1/3Nb2/3)0.2+x ]0.98Nb0.02O2.01, ZTMN) can be synthesized via a two-step solid state reaction method. The first calcination temperature is 1,300°C, and the second is not higher than 1,360°C. Incorporation of magnesium and niobium ions promotes the formation of the single phase solid solution with ZrTiO4 structure. Single phase perovskite PZTMN is formed at 780°C, much lower than that in conventional process. Dense ceramics can be sintered at about 1,260°C with dielectric and piezoelectric properties comparable to that of wet-dry method and higher than that of conventional method. It seems that B-site precursor method is cost effective in preparation of ternary piezoelectric ceramics. Springer Science+Business Media, LLC, 2006 Wu Yugong School of Electronic and Information Engineering, Tianjin University, 300072, Tianjin, People's Republic of China aut Wang Bin School of Electronic and Information Engineering, Tianjin University, 300072, Tianjin, People's Republic of China aut Cong Zhibo School of Electronic and Information Engineering, Tianjin University, 300072, Tianjin, People's Republic of China aut Wang Bu School of Electronic and Information Engineering, Tianjin University, 300072, Tianjin, People's Republic of China aut Journal of Materials Science Springer US; http://www.springer-ny.com 42/1(2007-01-01), 221-227 0022-2461 42:1<221 2007 42 10853 https://doi.org/10.1007/s10853-006-1055-y text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-006-1055-y text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Wu Yugong School of Electronic and Information Engineering, Tianjin University, 300072, Tianjin, People's Republic of China aut NATIONALLICENCE 700 1- Wang Bin School of Electronic and Information Engineering, Tianjin University, 300072, Tianjin, People's Republic of China aut NATIONALLICENCE 700 1- Cong Zhibo School of Electronic and Information Engineering, Tianjin University, 300072, Tianjin, People's Republic of China aut NATIONALLICENCE 700 1- Wang Bu School of Electronic and Information Engineering, Tianjin University, 300072, Tianjin, People's Republic of China aut NATIONALLICENCE 773 0- Journal of Materials Science Springer US; http://www.springer-ny.com 42/1(2007-01-01), 221-227 0022-2461 42:1<221 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer