caa a22 4500 463223632 CHVBK 20180405153220.0 cr unu---uuuuu 170326e20071001xx s 000 0 eng 10.1007/s10853-007-1761-0 doi (NATIONALLICENCE)springer-10.1007/s10853-007-1761-0 Effect of nanosized ferric oxide on the thermostability of methylsilicone resin [Elektronische Daten] [Chun-ying Min, Yu-dong Huang, Li Liu] Nanocomposite of methylsilicone resin/Fe2O3 (MSR/Fe2O3, metal oxide nanoparticles with average particle-size of 20nm) was successfully synthesized by acid-catalyzed hydrolysis and condensation of methyltrimethoxy silane (MTMS). The obtained nanocomposite was characterized by Fourier-transformed infrared (FT-IR) and X-ray photoelectron spectroscopy (XPS). The FTIR and XPS results show that the nanoparticles were well dispersed in the MSR matrix. The thermogravimetric analysis (TGA) results show that Fe2O3 nanoparticles can remarkably improve the thermal stability of MSR. In comparison with methylsilicone resin, the temperature values of the resulting nanocomposite at the onset of degradation and the maximum rate of mass loss were increased 55 and 76°C, respectively. Springer Science+Business Media, LLC, 2007 Min Chun-ying Polymer Materials and Engineering Division, Department of Applied Chemistry, Faculty of Science, Harbin Institute of Technology, P.O. Box 410, 150001, Harbin, P.R. China aut Huang Yu-dong Polymer Materials and Engineering Division, Department of Applied Chemistry, Faculty of Science, Harbin Institute of Technology, P.O. Box 410, 150001, Harbin, P.R. China aut Liu Li Polymer Materials and Engineering Division, Department of Applied Chemistry, Faculty of Science, Harbin Institute of Technology, P.O. Box 410, 150001, Harbin, P.R. China aut Journal of Materials Science Springer US; http://www.springer-ny.com 42/20(2007-10-01), 8695-8699 0022-2461 42:20<8695 2007 42 10853 https://doi.org/10.1007/s10853-007-1761-0 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-007-1761-0 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Min Chun-ying Polymer Materials and Engineering Division, Department of Applied Chemistry, Faculty of Science, Harbin Institute of Technology, P.O. Box 410, 150001, Harbin, P.R. China aut NATIONALLICENCE 700 1- Huang Yu-dong Polymer Materials and Engineering Division, Department of Applied Chemistry, Faculty of Science, Harbin Institute of Technology, P.O. Box 410, 150001, Harbin, P.R. China aut NATIONALLICENCE 700 1- Liu Li Polymer Materials and Engineering Division, Department of Applied Chemistry, Faculty of Science, Harbin Institute of Technology, P.O. Box 410, 150001, Harbin, P.R. China aut NATIONALLICENCE 773 0- Journal of Materials Science Springer US; http://www.springer-ny.com 42/20(2007-10-01), 8695-8699 0022-2461 42:20<8695 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer