caa a22 4500 463223810 CHVBK 20180405153220.0 cr unu---uuuuu 170326e20071001xx s 000 0 eng 10.1007/s10853-007-1807-3 doi (NATIONALLICENCE)springer-10.1007/s10853-007-1807-3 Preparation of Sb3Nb3O13 powders using molten salt method [Elektronische Daten] [Di Zhou, Hong Wang, Huanfu Zhou, Xiaojun Xie, Xi Yao, Yonghong Cheng] The powders of pure cubic phase of Sb3Nb3O13 were obtained using molten salt method at 1,100°C with incubation time of 3h. The formation of a kind of compound with hydroxyl restrains the volatilization and oxygenation of antimony oxides. The powder of cubic Sb3Nb3O13 shows octahedral shape and its size lies between 1μm and 20μm. Densified ceramic was obtained using the Sb3Nb3O13 powders. The microstructure of ceramic samples was studied by XRD and SEM analysis. And the dielectric properties as a function of frequency and temperature were measured between 25°C and 550°C and 100Hz∼1MHz. Springer Science+Business Media, LLC, 2007 Zhou Di Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education, Xi'an Jiaotong University, 710049, Xi'an, China aut Wang Hong Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education, Xi'an Jiaotong University, 710049, Xi'an, China aut Zhou Huanfu Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education, Xi'an Jiaotong University, 710049, Xi'an, China aut Xie Xiaojun State Key Laboratory of Electrical Insulation for Power Equipment, Xi'an Jiaotong University, 710049, Xi'an, China aut Yao Xi Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education, Xi'an Jiaotong University, 710049, Xi'an, China aut Cheng Yonghong State Key Laboratory of Electrical Insulation for Power Equipment, Xi'an Jiaotong University, 710049, Xi'an, China aut Journal of Materials Science Springer US; http://www.springer-ny.com 42/20(2007-10-01), 8387-8390 0022-2461 42:20<8387 2007 42 10853 https://doi.org/10.1007/s10853-007-1807-3 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-007-1807-3 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Zhou Di Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education, Xi'an Jiaotong University, 710049, Xi'an, China aut NATIONALLICENCE 700 1- Wang Hong Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education, Xi'an Jiaotong University, 710049, Xi'an, China aut NATIONALLICENCE 700 1- Zhou Huanfu Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education, Xi'an Jiaotong University, 710049, Xi'an, China aut NATIONALLICENCE 700 1- Xie Xiaojun State Key Laboratory of Electrical Insulation for Power Equipment, Xi'an Jiaotong University, 710049, Xi'an, China aut NATIONALLICENCE 700 1- Yao Xi Electronic Materials Research Laboratory, Key Laboratory of the Ministry of Education, Xi'an Jiaotong University, 710049, Xi'an, China aut NATIONALLICENCE 700 1- Cheng Yonghong State Key Laboratory of Electrical Insulation for Power Equipment, Xi'an Jiaotong University, 710049, Xi'an, China aut NATIONALLICENCE 773 0- Journal of Materials Science Springer US; http://www.springer-ny.com 42/20(2007-10-01), 8387-8390 0022-2461 42:20<8387 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer