caa a22 4500 463225678 CHVBK 20180405153226.0 cr unu---uuuuu 170326e20071101xx s 000 0 eng 10.1007/s10853-007-1866-5 doi (NATIONALLICENCE)springer-10.1007/s10853-007-1866-5 Preparation of meixnerite (Mg-Al-OH) type layered double hydroxide by a mechanochemical route [Elektronische Daten] [William Tongamp, Qiwu Zhang, Fumio Saito] We have attempted to synthesize the meixnerite (Mg-Al-OH) type layered double hydroxide (LDH) by a two step milling operation of a mixture of Mg(OH)2 and Al(OH)3 with water. In the first-step, a mixture of the starting materials was milled for 1h without water, and the product prepared in the first-step was milled for 2h with water in the second-step milling operation. The milled products were characterized by X-ray diffraction (XRD), Fourier transform infrared (FTIR), and thermo gravimetric-differential thermal analyses with mass spectroscopy (TG-DTA/MS). The surface morphology was characterized by scanning electron microscopy (SEM). Meixnerite with a small amount of carbonate was successfully synthesized mechanochemically at ambient conditions by milling for only 3h in a planetary ball mill. Springer Science+Business Media, LLC, 2007 Tongamp William Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1, Katahira, Aoba-Ku, 980-8577, Sendai, Japan aut Zhang Qiwu Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1, Katahira, Aoba-Ku, 980-8577, Sendai, Japan aut Saito Fumio Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1, Katahira, Aoba-Ku, 980-8577, Sendai, Japan aut Journal of Materials Science Springer US; http://www.springer-ny.com 42/22(2007-11-01), 9210-9215 0022-2461 42:22<9210 2007 42 10853 https://doi.org/10.1007/s10853-007-1866-5 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-007-1866-5 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Tongamp William Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1, Katahira, Aoba-Ku, 980-8577, Sendai, Japan aut NATIONALLICENCE 700 1- Zhang Qiwu Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1, Katahira, Aoba-Ku, 980-8577, Sendai, Japan aut NATIONALLICENCE 700 1- Saito Fumio Institute of Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1, Katahira, Aoba-Ku, 980-8577, Sendai, Japan aut NATIONALLICENCE 773 0- Journal of Materials Science Springer US; http://www.springer-ny.com 42/22(2007-11-01), 9210-9215 0022-2461 42:22<9210 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer