caa a22 4500 46322759X CHVBK 20180405153232.0 cr unu---uuuuu 170326e20070501xx s 000 0 eng 10.1007/s10853-006-1023-6 doi (NATIONALLICENCE)springer-10.1007/s10853-006-1023-6 A gas phase analysis technique applied to in-situ studies of gas-solid interactions [Elektronische Daten] [Clara Anghel, Qian Dong] An ultrahigh vacuum technique using mass spectrometry for in-situ investigations of gas-solid interactions is described in this paper. Examples of chemical reactions (oxidation, hydration) between solids and gas mixtures, dissociation of gases on solid surfaces, outgassing of solid materials and permeation of gases through membranes are discussed where the experimental arrangement is explained in detail. This Gas Phase Analysis (GPA) technique can be used at temperatures from room temperature to 1200°C and at pressures up to 1atm. Aspects related to sample preparation, isotopic gas mixture selection, data acquisition, calibration and interpretation of the experimental data are also addressed. Springer Science+Business Media, LLC, 2007 Anghel Clara Division of Corrosion Science, Department of Materials Science and Engineering, Royal Institute of Technology, Drottning Kristinas väg 51, 100 44, Stockholm, Sweden aut Dong Qian Division of Corrosion Science, Department of Materials Science and Engineering, Royal Institute of Technology, Drottning Kristinas väg 51, 100 44, Stockholm, Sweden aut Journal of Materials Science Springer US; http://www.springer-ny.com 42/10(2007-05-01), 3440-3453 0022-2461 42:10<3440 2007 42 10853 https://doi.org/10.1007/s10853-006-1023-6 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-006-1023-6 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Anghel Clara Division of Corrosion Science, Department of Materials Science and Engineering, Royal Institute of Technology, Drottning Kristinas väg 51, 100 44, Stockholm, Sweden aut NATIONALLICENCE 700 1- Dong Qian Division of Corrosion Science, Department of Materials Science and Engineering, Royal Institute of Technology, Drottning Kristinas väg 51, 100 44, Stockholm, Sweden aut NATIONALLICENCE 773 0- Journal of Materials Science Springer US; http://www.springer-ny.com 42/10(2007-05-01), 3440-3453 0022-2461 42:10<3440 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer