caa a22 4500 463228243 CHVBK 20180405153233.0 cr unu---uuuuu 170326e20070901xx s 000 0 eng 10.1007/s10853-007-1547-4 doi (NATIONALLICENCE)springer-10.1007/s10853-007-1547-4 Polyol-mediated synthesis of nanoscale Mg(OH)2 and MgO [Elektronische Daten] [Claus Feldmann, Susanne Matschulo, Sascha Ahlert] Nanoscale Mg(OH2) and MgO is prepared via a polyol-mediated synthesis. With concern to the experimental conditions, spherical particles, 20 and 100nm in size are realized. Dynamic light scattering proves the presence of non-agglomerated and monodispersed Mg(OH)2 in as-prepared suspensions of diethylene glycol. Based on the results of infrared spectroscopy, thermal analysis and X-ray powder diffraction, as-prepared Mg(OH)2 can be dehydrated at a surprisingly low temperature (300°C) to form MgO with almost similar particle size and shape. Springer Science+Business Media, LLC, 2007 Feldmann Claus Institut für Anorganische Chemie der Universität Karlsruhe (TH), Engesserstraße 15, 76131, Karlsruhe, Germany aut Matschulo Susanne Institut für Anorganische Chemie der Universität Karlsruhe (TH), Engesserstraße 15, 76131, Karlsruhe, Germany aut Ahlert Sascha K + S Aktiengesellschaft, Research and Development, Bertha-von-Suttner-Straße 7, 34111, Kassel, Germany aut Journal of Materials Science Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 42/17(2007-09-01), 7076-7080 0022-2461 42:17<7076 2007 42 10853 https://doi.org/10.1007/s10853-007-1547-4 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-007-1547-4 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Feldmann Claus Institut für Anorganische Chemie der Universität Karlsruhe (TH), Engesserstraße 15, 76131, Karlsruhe, Germany aut NATIONALLICENCE 700 1- Matschulo Susanne Institut für Anorganische Chemie der Universität Karlsruhe (TH), Engesserstraße 15, 76131, Karlsruhe, Germany aut NATIONALLICENCE 700 1- Ahlert Sascha K + S Aktiengesellschaft, Research and Development, Bertha-von-Suttner-Straße 7, 34111, Kassel, Germany aut NATIONALLICENCE 773 0- Journal of Materials Science Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 42/17(2007-09-01), 7076-7080 0022-2461 42:17<7076 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer