caa a22 4500 463232380 CHVBK 20180405153246.0 cr unu---uuuuu 170326e20071101xx s 000 0 eng 10.1007/s10853-007-1833-1 doi (NATIONALLICENCE)springer-10.1007/s10853-007-1833-1 Formation of surface magnetite nanoparticles from iron-exchanged zeolite using microwave radiation [Elektronische Daten] [J. Heuser, W. Spendel, A. Pisarenko, C. Yu, M. Pechan, G. Pacey] Microwave radiation simplifies synthesis methods by reducing reaction times, requiring fewer materials, and also controlling reaction processes. We have successfully synthesized nanoparticles of iron oxide and zinc oxide coated on zeolite A using microwaves. The radiation assisted in displacing either ferrous or zinc ions from the pre-loaded zeolite network and increasing reaction speed with solution at the interface. Products were characterized by TEM, XRD, VSM, ICP-AES, and fluorescence. We demonstrate the ability of using cation-exchanged zeolites as microreactors to bias reactions onto the zeolite surface. Efficient structure-directed surface reactions are a potential route to making unique supported nanomaterials for applications such as sensors, environmental remediation, and chemical catalysis. Springer Science+Business Media, LLC, 2007 Heuser J. Miami University Center for Nanotechnology, Department of Chemistry and Biochemistry, Miami University, 45056, Oxford, OH, USA aut Spendel W. Miami University Center for Nanotechnology, Department of Chemistry and Biochemistry, Miami University, 45056, Oxford, OH, USA aut Pisarenko A. Miami University Center for Nanotechnology, Department of Chemistry and Biochemistry, Miami University, 45056, Oxford, OH, USA aut Yu C. Department of Physics, Miami University, 45056, Oxford, OH, USA aut Pechan M. Department of Physics, Miami University, 45056, Oxford, OH, USA aut Pacey G. Miami University Center for Nanotechnology, Department of Chemistry and Biochemistry, Miami University, 45056, Oxford, OH, USA aut Journal of Materials Science Springer US; http://www.springer-ny.com 42/21(2007-11-01), 9057-9062 0022-2461 42:21<9057 2007 42 10853 https://doi.org/10.1007/s10853-007-1833-1 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-007-1833-1 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Heuser J. Miami University Center for Nanotechnology, Department of Chemistry and Biochemistry, Miami University, 45056, Oxford, OH, USA aut NATIONALLICENCE 700 1- Spendel W. Miami University Center for Nanotechnology, Department of Chemistry and Biochemistry, Miami University, 45056, Oxford, OH, USA aut NATIONALLICENCE 700 1- Pisarenko A. Miami University Center for Nanotechnology, Department of Chemistry and Biochemistry, Miami University, 45056, Oxford, OH, USA aut NATIONALLICENCE 700 1- Yu C. Department of Physics, Miami University, 45056, Oxford, OH, USA aut NATIONALLICENCE 700 1- Pechan M. Department of Physics, Miami University, 45056, Oxford, OH, USA aut NATIONALLICENCE 700 1- Pacey G. Miami University Center for Nanotechnology, Department of Chemistry and Biochemistry, Miami University, 45056, Oxford, OH, USA aut NATIONALLICENCE 773 0- Journal of Materials Science Springer US; http://www.springer-ny.com 42/21(2007-11-01), 9057-9062 0022-2461 42:21<9057 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer