caa a22 4500 463233689 CHVBK 20180405153250.0 cr unu---uuuuu 170326e20070601xx s 000 0 eng 10.1007/s10853-006-0402-3 doi (NATIONALLICENCE)springer-10.1007/s10853-006-0402-3 Malic acid complex method for preparation of LiNiVO4 nano-crystallites [Elektronische Daten] [Titipun Thongtem, Sulawan Kaowphong, Somchai Thongtem] LiNiVO4 nano-crystallites were prepared by the polymerized complex method using Li2CO3, Ni(CH3COO)2·4H2O and NH4VO3 as starting reagents and malic acid as a complexing agent. With the subsequent calcination at 450°C, the powder analyzed by XRD, FTIR, Raman, electron diffraction, SEM and TEM techniques was found to be inverse spinel LiNiVO4 with ∼20nm in diameter. TGA shows continuous weight loss at 40-450°C due to the evaporation and decomposition processes. Above 450°C, weight percent tended to be constant. In addition, formation mechanism of the purified LiNiVO4 was proposed to relate with the experimental results. Springer Science+Business Media, LLC, 2007 Thongtem Titipun Faculty of Science, Chiang Mai University, 50200, Chiang Mai, Thailand aut Kaowphong Sulawan Faculty of Science, Chiang Mai University, 50200, Chiang Mai, Thailand aut Thongtem Somchai Faculty of Science, Chiang Mai University, 50200, Chiang Mai, Thailand aut Journal of Materials Science Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 42/11(2007-06-01), 3923-3927 0022-2461 42:11<3923 2007 42 10853 https://doi.org/10.1007/s10853-006-0402-3 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-006-0402-3 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Thongtem Titipun Faculty of Science, Chiang Mai University, 50200, Chiang Mai, Thailand aut NATIONALLICENCE 700 1- Kaowphong Sulawan Faculty of Science, Chiang Mai University, 50200, Chiang Mai, Thailand aut NATIONALLICENCE 700 1- Thongtem Somchai Faculty of Science, Chiang Mai University, 50200, Chiang Mai, Thailand aut NATIONALLICENCE 773 0- Journal of Materials Science Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 42/11(2007-06-01), 3923-3927 0022-2461 42:11<3923 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer