caa a22 4500 463234383 CHVBK 20180405153252.0 cr unu---uuuuu 170326e20070801xx s 000 0 eng 10.1007/s10853-006-0673-8 doi (NATIONALLICENCE)springer-10.1007/s10853-006-0673-8 Investigation of solid solution of ZrP2O7-Sr2P2O7 [Elektronische Daten] [Semih Seyyidoğlu, Macit Özenbaş, Necmeddin Yazıcı, Ayşen Yılmaz] In this study, ZrP2O7 was synthesized by the solid state reaction of ZrO2 and NH4H2PO4 at 900°C. Then, in set 1; 10, 5, 1, 0.5, 0.1, 0.05, 0.03% previously prepared Sr2P2O7 were doped into ZrP2O7, and Sr2P2O7 slightly affect the unit cell parameter of cubic ZrP2O7 (a=8.248(6)-8.233(8)Å). The reverse of this process was also applied to Sr2P2O7 system (set 2). ZrP2O7 changes the unit cell parameters of orthorhombic Sr2P2O7 in between a=8.909(5)-8.877(5)Å, b=13.163(3)-13.12(1)Å, and c=5.403(2)-5.386(4)Å. Analysis of the vibrations of the P2O 7 4− ion and approximate band assignments for IR and Raman spectra are also reported in this work. Some coincidences in infrared and Raman spectra both sets were found and strong P-O-P bands were observed. Surface morphology, EDX analysis, and thermoluminescence properties of both sets were given the first time in this paper. Springer Science+Business Media, LLC, 2007 Seyyidoğlu Semih Department of Chemistry, Middle East Technical University, 06531, Ankara, Turkey aut Özenbaş Macit Department of Metallurgical and Materials Engineering, Middle East Technical University, 06531, Ankara, Turkey aut Yazıcı Necmeddin Department of Engineering Physics, Faculty of Engineering, Gaziantep University, 27310, Gaziantep, Turkey aut Yılmaz Ayşen Department of Chemistry, Middle East Technical University, 06531, Ankara, Turkey aut Journal of Materials Science Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 42/15(2007-08-01), 6453-6463 0022-2461 42:15<6453 2007 42 10853 https://doi.org/10.1007/s10853-006-0673-8 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10853-006-0673-8 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Seyyidoğlu Semih Department of Chemistry, Middle East Technical University, 06531, Ankara, Turkey aut NATIONALLICENCE 700 1- Özenbaş Macit Department of Metallurgical and Materials Engineering, Middle East Technical University, 06531, Ankara, Turkey aut NATIONALLICENCE 700 1- Yazıcı Necmeddin Department of Engineering Physics, Faculty of Engineering, Gaziantep University, 27310, Gaziantep, Turkey aut NATIONALLICENCE 700 1- Yılmaz Ayşen Department of Chemistry, Middle East Technical University, 06531, Ankara, Turkey aut NATIONALLICENCE 773 0- Journal of Materials Science Kluwer Academic Publishers-Plenum Publishers; http://www.springer-ny.com 42/15(2007-08-01), 6453-6463 0022-2461 42:15<6453 2007 42 10853 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer