caa a22 4500 463239679 CHVBK 20180405153309.0 cr unu---uuuuu 170326e20070501xx s 000 0 eng 10.1007/s10947-007-0079-8 doi (NATIONALLICENCE)springer-10.1007/s10947-007-0079-8 Crystal and molecular structure of 1,3,4,6-etraphenylimidazolio[4,5- d ]-imidazolium bis(phenylenedioxytetrachlorophosphate) [Elektronische Daten] [E. Mironova, A. Gubaidullin, I. Litvinov, V. Mironov, A. Shtyrlina, V. Kovalenko, R. Shagidullin] X-ray diffraction structural study of a novel aromatic 10π-electron system of 1,3,4,6-tetraphenyl-imidazolio[4,5-d]-imidazolium bis(phenylenedioxytetrachlorophosphate) is carried out. The crystals are monoclinic; a = 8.483(2) Å, b = 23.986(4) Å, c = 10.727(2) Å; β = 106.84(2)°; V = 2089.1(7) Å3, space group P21/n. The compound crystallizes as a salt containing two phenylenedioxytetrachlorophoshate anions per one dication of 1,3,4,6-tetraphenylimidazolio[4,5-d]imidazolium. The cation occupies a special position on the inversion center. There are short C-H...X (X = O, Cl) contacts and π-π-interactions between aromatic fragments in the crystal and their combined effect results in the development of a layered structure. Springer Science+Business Media, Inc., 2007 1,3,4,6-tetraphenylimidazolio[4,5- d ]-imidazolium bis(phenylenedioxytetrachlorophosphate) nationallicence crystal and molecular structure nationallicence X-ray diffraction analysis nationallicence Mironova E. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut Gubaidullin A. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut Litvinov I. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut Mironov V. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut Shtyrlina A. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut Kovalenko V. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut Shagidullin R. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut Journal of Structural Chemistry Springer US 48/3(2007-05-01), 528-533 0022-4766 48:3<528 2007 48 10947 https://doi.org/10.1007/s10947-007-0079-8 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10947-007-0079-8 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Mironova E. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut NATIONALLICENCE 700 1- Gubaidullin A. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut NATIONALLICENCE 700 1- Litvinov I. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut NATIONALLICENCE 700 1- Mironov V. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut NATIONALLICENCE 700 1- Shtyrlina A. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut NATIONALLICENCE 700 1- Kovalenko V. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut NATIONALLICENCE 700 1- Shagidullin R. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Scientific Center, Russian Academy of Sciences, Kazan aut NATIONALLICENCE 773 0- Journal of Structural Chemistry Springer US 48/3(2007-05-01), 528-533 0022-4766 48:3<528 2007 48 10947 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer