caa a22 4500 465749100 CHVBK 20180323111828.0 cr unu---uuuuu 170327e19900101xx s 000 0 eng 10.1007/BF00322527 doi (NATIONALLICENCE)springer-10.1007/BF00322527 Preparation and analysis of a marine sediment reference material for the determination of trace organic constituents [Elektronische Daten] [Michele Schantz, Bruce Benner Jr., Stephen Chesler, Barbara Koster, Karen Hehn, Susan Stone, W. Kelly, Rolf Zeisler, Stephen Wise] Summary: A new marine sediment Standard Reference Material (SRM) has been prepared and analyzed for the determination of trace organic constituents. SRM 1941, Organics in Marine Sediment, has been certified for concentrations of 11 PAHs using results obtained from gas chromatography (GC) with flame ionization detection, gas chromatography-mass spectrometry, and liquid chromatography with fluorescence detection. Non-certified values for 24 additional PAHs are also reported. GC with electron capture detection was used to provide non-certified concentrations for 15 PCB congeners and 7 chlorinated pesticides. In addition to the organic contaminants, concentrations of 32 major and trace elements were determined using neutron activation analysis, and the sulfur content was also determined using isotope dilution thermal ionization mass spectrometry. Springer-Verlag, 1990 Schantz Michele Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Benner Jr. Bruce Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Chesler Stephen Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Koster Barbara Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Hehn Karen Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Stone Susan Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Kelly W. Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Zeisler Rolf Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Wise Stephen Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut Fresenius' Journal of Analytical Chemistry Springer-Verlag 338/4(1990-01-01), 501-514 0937-0633 338:4<501 1990 338 216 https://doi.org/10.1007/BF00322527 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/BF00322527 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Schantz Michele Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 700 1- Benner Jr Bruce Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 700 1- Chesler Stephen Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 700 1- Koster Barbara Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 700 1- Hehn Karen Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 700 1- Stone Susan Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 700 1- Kelly W. Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 700 1- Zeisler Rolf Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 700 1- Wise Stephen Center for Analytical Chemistry, National Institute of Standards and Technology, 20899, Gaithersburg, MD, USA aut NATIONALLICENCE 773 0- Fresenius' Journal of Analytical Chemistry Springer-Verlag 338/4(1990-01-01), 501-514 0937-0633 338:4<501 1990 338 216 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer