caa a22 4500 467926476 CHVBK 20180406152931.0 cr unu---uuuuu 170328e20060301xx s 000 0 eng 10.1134/S0020168506030071 doi (NATIONALLICENCE)springer-10.1134/S0020168506030071 Preparation of Ti3SiC2 [Elektronische Daten] [P. Istomin, A. Nadutkin, Yu. Ryabkov, B. Goldin] Phase relations in the Ti-C-SiC system are studied with the aim of optimizing Ti3SiC2 synthesis. The optimal starting-mixture compositions for the synthesis of phase-pure Ti3SiC2 powder can be represented by the formula 3Ti + (1 − z)C + (1 + z)SiC, where z = 0.2-0.6. In the temperature range 1630-1670 K under dynamic vacuum, the excess silicon vaporizes from the sample. The processes leading to the formation of impurity phases are discussed. Pleiades Publishing, Inc., 2006 Istomin P. Institute of Chemistry, Komi Scientific Center, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 48, 167982, Syktyvkar, Komi Republic, Russia aut Nadutkin A. Institute of Chemistry, Komi Scientific Center, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 48, 167982, Syktyvkar, Komi Republic, Russia aut Ryabkov Yu Institute of Chemistry, Komi Scientific Center, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 48, 167982, Syktyvkar, Komi Republic, Russia aut Goldin B. Institute of Chemistry, Komi Scientific Center, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 48, 167982, Syktyvkar, Komi Republic, Russia aut Inorganic Materials Nauka/Interperiodica 42/3(2006-03-01), 250-255 0020-1685 42:3<250 2006 42 10789 https://doi.org/10.1134/S0020168506030071 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1134/S0020168506030071 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Istomin P. Institute of Chemistry, Komi Scientific Center, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 48, 167982, Syktyvkar, Komi Republic, Russia aut NATIONALLICENCE 700 1- Nadutkin A. Institute of Chemistry, Komi Scientific Center, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 48, 167982, Syktyvkar, Komi Republic, Russia aut NATIONALLICENCE 700 1- Ryabkov Yu Institute of Chemistry, Komi Scientific Center, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 48, 167982, Syktyvkar, Komi Republic, Russia aut NATIONALLICENCE 700 1- Goldin B. Institute of Chemistry, Komi Scientific Center, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 48, 167982, Syktyvkar, Komi Republic, Russia aut NATIONALLICENCE 773 0- Inorganic Materials Nauka/Interperiodica 42/3(2006-03-01), 250-255 0020-1685 42:3<250 2006 42 10789 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer