caa a22 4500 467926859 CHVBK 20180406152932.0 cr unu---uuuuu 170328e20061001xx s 000 0 eng 10.1134/S0020168506100141 doi (NATIONALLICENCE)springer-10.1134/S0020168506100141 Preparation of MnCo2O4 whiskers and spheroids through thermal decomposition of Mn1/3Co2/3C2O4 · 2H2O [Elektronische Daten] [O. Gyrdasova, G. Bazuev, I. Grigorov, O. Koryakova] The mixed oxalate Mn1/3Co2/3C2O4 · 2H2O has been prepared in the form of whiskers 2-5 μm in diameter and up to 50 μm in length and spheroidal nanofiber arrays 20 μm in diameter using two different coprecipitation procedures. Thermal decomposition of this oxalate in air has led to the formation of MnCo2O4 particles very similar in morphology to their oxalate precursor. The materials have been characterized by chemical analysis, thermogravimetry, x-ray diffraction. IR spectroscopy, and scanning electron microscopy. Pleiades Publishing, Inc., 2006 Gyrdasova O. Institute of Solid-State Chemistry, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 91, 620219, Yekaterinburg, Russia aut Bazuev G. Institute of Solid-State Chemistry, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 91, 620219, Yekaterinburg, Russia aut Grigorov I. Institute of Solid-State Chemistry, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 91, 620219, Yekaterinburg, Russia aut Koryakova O. Institute of Solid-State Chemistry, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 91, 620219, Yekaterinburg, Russia aut Inorganic Materials Nauka/Interperiodica 42/10(2006-10-01), 1126-1132 0020-1685 42:10<1126 2006 42 10789 https://doi.org/10.1134/S0020168506100141 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1134/S0020168506100141 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Gyrdasova O. Institute of Solid-State Chemistry, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 91, 620219, Yekaterinburg, Russia aut NATIONALLICENCE 700 1- Bazuev G. Institute of Solid-State Chemistry, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 91, 620219, Yekaterinburg, Russia aut NATIONALLICENCE 700 1- Grigorov I. Institute of Solid-State Chemistry, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 91, 620219, Yekaterinburg, Russia aut NATIONALLICENCE 700 1- Koryakova O. Institute of Solid-State Chemistry, Ural Division, Russian Academy of Sciences, Pervomaiskaya ul. 91, 620219, Yekaterinburg, Russia aut NATIONALLICENCE 773 0- Inorganic Materials Nauka/Interperiodica 42/10(2006-10-01), 1126-1132 0020-1685 42:10<1126 2006 42 10789 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer