caa a22 4500 467927499 CHVBK 20180406152933.0 cr unu---uuuuu 170328e20060501xx s 000 0 eng 10.1134/S0020168506050177 doi (NATIONALLICENCE)springer-10.1134/S0020168506050177 Synthesis and recycling of lead tungstate [Elektronische Daten] [V. Kalinnikov, O. Gromov, A. Kuz'min, G. Kunshina, E. Lokshin, Yu. Savel'ev, S. Burachas] We have developed liquid-phase and solid-state processes for the preparation of tetragonal lead tungstate powder with the stoichiometric PbO: WO3 ratio. Solid-state synthesis has been shown to have a number of significant advantages over the liquid-phase process. In addition, a procedure has been developed for processing PbWO4 crystal growth waste through PbWO4 decomposition in nitric acid, which ensures the preparation of extrapure-grade WO3 and PbO. The WO3 and PbO thus obtained have been used in solid-state synthesis of PbWO4, from which high-quality crystals have been grown. Pleiades Publishing, Inc., 2006 Kalinnikov V. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut Gromov O. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut Kuz'min A. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut Kunshina G. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut Lokshin E. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut Savel'ev Yu OAO Severnye Kristally, Promploshchadka 3, 184200, Apatity, Murmansk oblast, Russia aut Burachas S. OAO Severnye Kristally, Promploshchadka 3, 184200, Apatity, Murmansk oblast, Russia aut Inorganic Materials Nauka/Interperiodica 42/5(2006-05-01), 543-549 0020-1685 42:5<543 2006 42 10789 https://doi.org/10.1134/S0020168506050177 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1134/S0020168506050177 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Kalinnikov V. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut NATIONALLICENCE 700 1- Gromov O. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut NATIONALLICENCE 700 1- Kuz'min A. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut NATIONALLICENCE 700 1- Kunshina G. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut NATIONALLICENCE 700 1- Lokshin E. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Scientific Center, Russian Academy of Sciences, ul. Fersmana 26a, 184209, Apatity, Murmansk oblast, Russia aut NATIONALLICENCE 700 1- Savel'ev Yu OAO Severnye Kristally, Promploshchadka 3, 184200, Apatity, Murmansk oblast, Russia aut NATIONALLICENCE 700 1- Burachas S. OAO Severnye Kristally, Promploshchadka 3, 184200, Apatity, Murmansk oblast, Russia aut NATIONALLICENCE 773 0- Inorganic Materials Nauka/Interperiodica 42/5(2006-05-01), 543-549 0020-1685 42:5<543 2006 42 10789 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer