caa a22 4500 467952507 CHVBK 20180405193743.0 cr unu---uuuuu 170328e20050101xx s 000 0 eng 10.1007/s10809-005-0018-9 doi (NATIONALLICENCE)springer-10.1007/s10809-005-0018-9 (NATIONALLICENCE)springer-10.1007/s10809-005-0061-6 A test method for determining palladium in chloride solutions on the solid phase of a fibrous anion exchanger [Elektronische Daten] [V. Dedkova, O. Shvoeva, S. Savvin] The sorption of palladium(II) from chloride solutions on polyacrylonitrile fiber filled with the AV-17 anion exchanger (PANF-AV-17) and its subsequent determination with p-nitrosodiethylaniline on the solid phase were studied. The results of determining palladium with this reagent on the solid phase of polyacrylonitrile fiber filled with the KU-2 cation exchanger and the AV-17 anion exchanger were compared. A test method was developed for determining palladium on the PANF-AV-17 solid phase. Sorption was performed in the batch mode; the analytical signal was estimated by measuring the diffuse reflection coefficient or visually using a color scale. The detection limit was 0.005 µg/mL; the range of the calibration scale was 0-0.2 µg/mL at the volume of the test solution 10-20 mL. The accuracy of the procedure was verified by the added-found method in the analysis of tap water and a standard reference sample of natural sodium chloride water. The relative standard deviation was no more than 25%; the time of the analysis of 5 or 6 samples was 25-30 min. Pleiades Publishing, Inc., 2005 Dedkova V. Vernadsky Institute of Geochemistry and Analytical Chemistry, ul. Kosygina 19, 119991, Moscow, Russia aut Shvoeva O. Vernadsky Institute of Geochemistry and Analytical Chemistry, ul. Kosygina 19, 119991, Moscow, Russia aut Savvin S. Vernadsky Institute of Geochemistry and Analytical Chemistry, ul. Kosygina 19, 119991, Moscow, Russia aut Journal of Analytical Chemistry Nauka/Interperiodica 60/1(2005-01-01), 75-79 1061-9348 60:1<75 2005 60 10809 https://doi.org/10.1007/s10809-005-0018-9 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10809-005-0018-9 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Dedkova V. Vernadsky Institute of Geochemistry and Analytical Chemistry, ul. Kosygina 19, 119991, Moscow, Russia aut NATIONALLICENCE 700 1- Shvoeva O. Vernadsky Institute of Geochemistry and Analytical Chemistry, ul. Kosygina 19, 119991, Moscow, Russia aut NATIONALLICENCE 700 1- Savvin S. Vernadsky Institute of Geochemistry and Analytical Chemistry, ul. Kosygina 19, 119991, Moscow, Russia aut NATIONALLICENCE 773 0- Journal of Analytical Chemistry Nauka/Interperiodica 60/1(2005-01-01), 75-79 1061-9348 60:1<75 2005 60 10809 NATIONALLICENCE 700 1- Dedkova V. Vernadsky Institute of Geochemistry and Analytical Chemistry, Russian Academy of Sciences, ul. Kosygina 19, 119991, Moscow, Russia aut NATIONALLICENCE 700 1- Shvoeva O. Vernadsky Institute of Geochemistry and Analytical Chemistry, Russian Academy of Sciences, ul. Kosygina 19, 119991, Moscow, Russia aut NATIONALLICENCE 700 1- Savvin S. Vernadsky Institute of Geochemistry and Analytical Chemistry, Russian Academy of Sciences, ul. Kosygina 19, 119991, Moscow, Russia aut NATIONALLICENCE 856 40 https://doi.org/10.1007/s10809-005-0061-6 text/html Onlinezugriff via DOI Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer NATIONALLICENCE NATIONALLICENCE NL-springer