caa a22 4500 467954542 CHVBK 20180405193745.0 cr unu---uuuuu 170328e20050201xx s 000 0 eng 10.1007/s10809-005-0034-9 doi (NATIONALLICENCE)springer-10.1007/s10809-005-0034-9 (NATIONALLICENCE)springer-10.1007/PL00021914 Characterization of the interlaboratory reproducibility of results in quantitative gas-chromatographic analysis using the internal normalization method [Elektronische Daten] [I. Zenkevich, A. Eshchenko, I. Klimova] A comparison of the results of gas-chromatographic analysis performed for the same samples with the use of various instruments with flame-ionization detectors and different (packed and capillary) columns indicates statistically significant differences in the results of data processing by the internal normalization method. Such variations in relative peak areas were detected on the same instrument on a comparison between data obtained under isothermal conditions and with temperature programming. Conceivable reasons for the observed changes in relative peak areas and procedures for the evaluation of errors due to this effect in the analysis of various samples on particular instruments are considered. MAIK "Nauka/Interperiodica”, 2005 Zenkevich I. Chemistry Research Institute, St. Petersburg State University, Universitetskii pr. 26, 198504, Petrodvorets, Russia aut Eshchenko A. Department of Chemistry, St. Petersburg State University (Petrodvorets Branch), Universitetskii pr. 2, 198904, Petrodvorets, Russia aut Klimova I. Chemistry Research Institute, St. Petersburg State University, Universitetskii pr. 26, 198504, Petrodvorets, Russia aut Journal of Analytical Chemistry Nauka/Interperiodica 60/2(2005-02-01), 119-124 1061-9348 60:2<119 2005 60 10809 https://doi.org/10.1007/s10809-005-0034-9 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s10809-005-0034-9 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Zenkevich I. Chemistry Research Institute, St. Petersburg State University, Universitetskii pr. 26, 198504, Petrodvorets, Russia aut NATIONALLICENCE 700 1- Eshchenko A. Department of Chemistry, St. Petersburg State University (Petrodvorets Branch), Universitetskii pr. 2, 198904, Petrodvorets, Russia aut NATIONALLICENCE 700 1- Klimova I. Chemistry Research Institute, St. Petersburg State University, Universitetskii pr. 26, 198504, Petrodvorets, Russia aut NATIONALLICENCE 773 0- Journal of Analytical Chemistry Nauka/Interperiodica 60/2(2005-02-01), 119-124 1061-9348 60:2<119 2005 60 10809 NATIONALLICENCE 856 40 https://doi.org/10.1007/PL00021914 text/html Onlinezugriff via DOI Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer NATIONALLICENCE NATIONALLICENCE NL-springer