caa a22 4500 469037997 CHVBK 20180323132800.0 cr unu---uuuuu 170328e19921201xx s 000 0 eng 10.1007/BF00808271 doi (NATIONALLICENCE)springer-10.1007/BF00808271 Synthesis and characterization of Co(II), Ni(II), and Cu(II) complexes of salicylal-4-aminoantipyrine and 2-hydroxy-1-naphthol-4-aminoantipyrine and their adducts [Elektronische Daten] [Mohamed Gaber, Hassan Mabrouk, Abd Ba-Issa, Mohamed Ayad] Synthese und Charakterisierung von Co(II), Ni(II) und Cu(II)-Komplexen von Salicylal-4-aminoantipyrinen und 2-Hydroxy-1-naphthol-4-aminoantipyrinen und ihren Addukten Summary: The electrochemical oxidation of anodic Co, Ni and Cu in acetone solutions of 4-aminoantipyrine Schiff base of salicyaldehyde (SAAP) and 2-hydroxy-1-naphthaldehyde (NAAP) [=R(OH)] gave the title complexes in high yields. When neutral mono- or bidentate donors were present in the solution, the products were the 1:1 adducts of mixed complexes. The complexes were characterized by elemental analysis, IR, electronic, and ESR spectra as well as magnetic moment measurements. The thermal (DTA) behaviour and electrical properties of some complexes were investigated in the solid state and correlated with the structure of the complexes. Springer-Verlag, 1992 Electrochemistry nationallicence Transition metals nationallicence Schiff base nationallicence Complexes nationallicence Gaber Mohamed Chemistry Department, Faculty of Science, Sana'a University, Sana'a P.O. Box 11503, Yemen aut Mabrouk Hassan Chemistry Department, Faculty of Science, Sana'a University, Sana'a P.O. Box 11503, Yemen aut Ba-Issa Abd Chemistry Department, Faculty of Science, Sana'a University, Sana'a P.O. Box 11503, Yemen aut Ayad Mohamed Chemistry Department, Faculty of Science, Tanta University, Tanta, Egypt aut Monatshefte für Chemie / Chemical Monthly Springer-Verlag 123/12(1992-12-01), 1089-1097 0026-9247 123:12<1089 1992 123 706 https://doi.org/10.1007/BF00808271 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/BF00808271 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Gaber Mohamed Chemistry Department, Faculty of Science, Sana'a University, Sana'a P.O. Box 11503, Yemen aut NATIONALLICENCE 700 1- Mabrouk Hassan Chemistry Department, Faculty of Science, Sana'a University, Sana'a P.O. Box 11503, Yemen aut NATIONALLICENCE 700 1- Ba-Issa Abd Chemistry Department, Faculty of Science, Sana'a University, Sana'a P.O. Box 11503, Yemen aut NATIONALLICENCE 700 1- Ayad Mohamed Chemistry Department, Faculty of Science, Tanta University, Tanta, Egypt aut NATIONALLICENCE 773 0- Monatshefte für Chemie / Chemical Monthly Springer-Verlag 123/12(1992-12-01), 1089-1097 0026-9247 123:12<1089 1992 123 706 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer