caa a22 4500 469058099 CHVBK 20180323132849.0 cr unu---uuuuu 170328e19920901xx s 000 0 eng 10.1007/BF00547620 doi (NATIONALLICENCE)springer-10.1007/BF00547620 Identification and quantitative determination of low-molecular-weight compounds and precipitation and plasticizing baths, and the effect of monomer-and solvent-contamination on their composition [Elektronische Daten] [T. Podol'skaya, P. Smirnov, N. Kuz'min, K. Khabarova, N. Kvasha, A. Chegolya] Conclusions: -- Using the liquid-chromatography method, a selective procedure has been developed for the quantitative determination of low-molecular compounds in the precipitation bath and the plasticizing bath. -- Identification of the PB composition. It has been shown that the low-molecular compounds evolved into the PB are not linear oligomers but polymetaphenylene isophthalamide, and presumptively, they have a cyclic structure. -- The effect of contaminants in isophthaloyl chloride and in dimethylacetamide on the quantitative and qualitative composition of the PB and P/B has been studied. -- It has been established that the main contaminants which affect the composition of PB are isophthalic and acetic acids. Plenum Publishing Corporation, 1992 Podol'skaya T. aut Smirnov P. aut Kuz'min N. aut Khabarova K. aut Kvasha N. aut Chegolya A. aut Fibre Chemistry Kluwer Academic Publishers-Plenum Publishers 23/5(1992-09-01), 371-374 0015-0541 23:5<371 1992 23 10692 https://doi.org/10.1007/BF00547620 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/BF00547620 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Podol'skaya T. aut NATIONALLICENCE 700 1- Smirnov P. aut NATIONALLICENCE 700 1- Kuz'min N. aut NATIONALLICENCE 700 1- Khabarova K. aut NATIONALLICENCE 700 1- Kvasha N. aut NATIONALLICENCE 700 1- Chegolya A. aut NATIONALLICENCE 773 0- Fibre Chemistry Kluwer Academic Publishers-Plenum Publishers 23/5(1992-09-01), 371-374 0015-0541 23:5<371 1992 23 10692 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer