caa a22 4500 469059400 CHVBK 20180323132852.0 cr unu---uuuuu 170328e19920501xx s 000 0 eng 10.1007/BF01076674 doi (NATIONALLICENCE)springer-10.1007/BF01076674 Inclusion of multi-ring compounds by p-tert -butylcalix[5]arene [Elektronische Daten] [Ravindra Juneja, Kerry Robinson, G. William Orr, Raymond Dubois, Kenneth Belmore, Jerry Atwood, John Ripmeester, Christopher Ratcliffe] The inclusion complex ofp-tert-butylcalix[5]arene with tetralin has been characterized in the solid state by a single crystal X-ray diffraction study and by13C CP/MAS NMR experiments. A crystallographic mirror plane bisects the calix[5]arene and contains the tetralin molecule (which is dynamically disordered). The guest penetrates the upper rim of the calixarene and the experimental results indicate the saturated ring is imbedded most deeply.p-tert-Butylcalix[5]arene (tetralin) · 2 EtOH belongs to the monoclinic space group C2/m witha = 22.187(6),b = 15.823(6),c = 18.168(5) Å,β = 99.70(2)°, andD c = 1.09 g cm−3 forZ = 4. Refinement based on 1652 observed reflections led to a finalR value of 0.081. Kluwer Academic Publishers, 1992 Calix[5]arene nationallicence multi-ring compound nationallicence tetralin nationallicence solid state NMR nationallicence X-ray diffraction nationallicence Juneja Ravindra Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut Robinson Kerry Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut William Orr G. Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut Dubois Raymond Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut Belmore Kenneth Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut Atwood Jerry Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut Ripmeester John Steacie Institute for Molecular Sciences, National Research Council of Canada, KIA OR9, Ottawa, Ontario, Canada aut Ratcliffe Christopher Steacie Institute for Molecular Sciences, National Research Council of Canada, KIA OR9, Ottawa, Ontario, Canada aut Journal of inclusion phenomena and molecular recognition in chemistry Kluwer Academic Publishers 13/1(1992-05-01), 93-96 0923-0750 13:1<93 1992 13 10847 https://doi.org/10.1007/BF01076674 text/html Onlinezugriff via DOI 1 brief-communication jats NATIONALLICENCE 856 40 https://doi.org/10.1007/BF01076674 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Juneja Ravindra Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut NATIONALLICENCE 700 1- Robinson Kerry Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut NATIONALLICENCE 700 1- William Orr G. Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut NATIONALLICENCE 700 1- Dubois Raymond Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut NATIONALLICENCE 700 1- Belmore Kenneth Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut NATIONALLICENCE 700 1- Atwood Jerry Department of Chemistry, University of Alabama, 35487, Tuscaloosa, AL, USA aut NATIONALLICENCE 700 1- Ripmeester John Steacie Institute for Molecular Sciences, National Research Council of Canada, KIA OR9, Ottawa, Ontario, Canada aut NATIONALLICENCE 700 1- Ratcliffe Christopher Steacie Institute for Molecular Sciences, National Research Council of Canada, KIA OR9, Ottawa, Ontario, Canada aut NATIONALLICENCE 773 0- Journal of inclusion phenomena and molecular recognition in chemistry Kluwer Academic Publishers 13/1(1992-05-01), 93-96 0923-0750 13:1<93 1992 13 10847 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer