caa a22 4500 469059524 CHVBK 20180323132853.0 cr unu---uuuuu 170328e19920701xx s 000 0 eng 10.1007/BF01042784 doi (NATIONALLICENCE)springer-10.1007/BF01042784 Preparation and properties of insoluble films of cyclodextrin condensation polymers [Elektronische Daten] [Wlodzimierz Kutner, Winfried Storck, Karl Doblhofer] The preparation and properties of smooth and stable films of cyclodextrin polymers are described. The commercially available water soluble prepolymers ofα-, β-, andγ-cyclodextrin of low molecular masses were crosslinked with glutaric dialdehyde. Side-chain unreacted aldehyde groups were reduced with sodium borohydride. For theα-cyclodextrin polymer, optimum film performance was found for a 1:10 mass ratio of glutaric dialdehyde to prepolymer, which corresponds to a molar ratio of glutaric dialdehyde to cyclodextrin units of about 1.75: 1. Such films, of thickness 2.4 µm, were prepared on metallic or glassy-carbon substrates for characterization by scanning-electron microscopy, and for studies with the electrochemical quartz-crystal microbalance. Kluwer Academic Publishers, 1992 Cyclodextrin polymer film nationallicence polymer modified electrode nationallicence membrane nationallicence polycondensation nationallicence electrochemical quartz-crystal microbalance nationallicence Kutner Wlodzimierz Fritz-Haber-Institut der Max-Planck-Gesellschaft, Faradayweg 4-6, D-W-1000, Berlin 33, Germany aut Storck Winfried Fritz-Haber-Institut der Max-Planck-Gesellschaft, Faradayweg 4-6, D-W-1000, Berlin 33, Germany aut Doblhofer Karl Fritz-Haber-Institut der Max-Planck-Gesellschaft, Faradayweg 4-6, D-W-1000, Berlin 33, Germany aut Journal of inclusion phenomena and molecular recognition in chemistry Kluwer Academic Publishers 13/3(1992-07-01), 257-265 0923-0750 13:3<257 1992 13 10847 https://doi.org/10.1007/BF01042784 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/BF01042784 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Kutner Wlodzimierz Fritz-Haber-Institut der Max-Planck-Gesellschaft, Faradayweg 4-6, D-W-1000, Berlin 33, Germany aut NATIONALLICENCE 700 1- Storck Winfried Fritz-Haber-Institut der Max-Planck-Gesellschaft, Faradayweg 4-6, D-W-1000, Berlin 33, Germany aut NATIONALLICENCE 700 1- Doblhofer Karl Fritz-Haber-Institut der Max-Planck-Gesellschaft, Faradayweg 4-6, D-W-1000, Berlin 33, Germany aut NATIONALLICENCE 773 0- Journal of inclusion phenomena and molecular recognition in chemistry Kluwer Academic Publishers 13/3(1992-07-01), 257-265 0923-0750 13:3<257 1992 13 10847 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer