caa a22 4500 475760964 CHVBK 20180406123551.0 cr unu---uuuuu 170329e20000401xx s 000 0 eng 10.1007/BF02495493 doi (NATIONALLICENCE)springer-10.1007/BF02495493 Synthesis, structure, and properties of piperidinium 3-(4-chlorophenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)thiopropionimidate [Elektronische Daten] [S. Krivokolysko, V. Dyachenko, A. Chernega, V. Litvinov] Condensation of 4-chlorobenzaldehyde with cyanothioacetamide and dimedone in the presence of piperidine afforded piperidinium 3-(4-chlorophenyl)-2-cyano-3-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)thiopropionimidate. This salt was studied by X-ray diffraction analysis and used in the synthesis of the previously unknown partially hydrogenated 2-alkylthioquinolin-2-ones. Kluwer Academic/Plenum Publishers, 2000 condensation nationallicence 4-chlorobenzaldehyde nationallicence dimedone nationallicence cyanothioacetamide nationallicence cyclohexen-1-ol nationallicence quinolinones nationallicence alkylation nationallicence X-ray diffraction analysis nationallicence Krivokolysko S. Taras Shevchenko Lugansk State Pedagogical University, 2 ul. Oboronnaya, 91011, Lugansk, Ukraine aut Dyachenko V. Taras Shevchenko Lugansk State Pedagogical University, 2 ul. Oboronnaya, 91011, Lugansk, Ukraine aut Chernega A. Institute of Organic Chemistry, Ukrainian National Academy of Sciences, 5 ul. Murmanskaya, 253660, Kiev, Ukraine aut Litvinov V. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 117913, Moscow, Russian Federation aut Russian Chemical Bulletin Kluwer Academic Publishers-Plenum Publishers 49/4(2000-04-01), 736-739 1066-5285 49:4<736 2000 49 11172 https://doi.org/10.1007/BF02495493 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/BF02495493 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Krivokolysko S. Taras Shevchenko Lugansk State Pedagogical University, 2 ul. Oboronnaya, 91011, Lugansk, Ukraine aut NATIONALLICENCE 700 1- Dyachenko V. Taras Shevchenko Lugansk State Pedagogical University, 2 ul. Oboronnaya, 91011, Lugansk, Ukraine aut NATIONALLICENCE 700 1- Chernega A. Institute of Organic Chemistry, Ukrainian National Academy of Sciences, 5 ul. Murmanskaya, 253660, Kiev, Ukraine aut NATIONALLICENCE 700 1- Litvinov V. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 117913, Moscow, Russian Federation aut NATIONALLICENCE 773 0- Russian Chemical Bulletin Kluwer Academic Publishers-Plenum Publishers 49/4(2000-04-01), 736-739 1066-5285 49:4<736 2000 49 11172 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer