caa a22 4500 475761839 CHVBK 20180406123553.0 cr unu---uuuuu 170329e20000201xx s 000 0 eng 10.1007/BF02494678 doi (NATIONALLICENCE)springer-10.1007/BF02494678 Cyclic phosphorochloridites (chloridates) based on chiral butane-2,3-diol and dihydrobenzoin as reagents for the analysis of enantiomeric compositions of alcohols by31P NMR spectroscopy [Elektronische Daten] [A. Bredikhin, Z. Bredikhina, L. Gaisina, E. Strunskaya, N. Azancheev] The use of cyclic phosphorochloridites which were prepared based on PCl3 and chiral butane-2,3-diol or hydrobenzoin as possible reagents for the analysis of the enantiomeric composition of chiral alcohols by31P NMR spectroscopy is considered. The diastereomeric dispersion of chemical shifts of the resulting phosphites as well as of derived phosphates and thiophosphates is compared with that of structurally similar reagents. Kluwer Academic/Plenum Publishers, 2000 C 2-symmetrical chiral diols nationallicence chiral alcohols nationallicence enantiomeric composition nationallicence 31P NMR spectra nationallicence Bredikhin A. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut Bredikhina Z. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut Gaisina L. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut Strunskaya E. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut Azancheev N. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut Russian Chemical Bulletin Kluwer Academic Publishers-Plenum Publishers 49/2(2000-02-01), 310-313 1066-5285 49:2<310 2000 49 11172 https://doi.org/10.1007/BF02494678 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/BF02494678 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Bredikhin A. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut NATIONALLICENCE 700 1- Bredikhina Z. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut NATIONALLICENCE 700 1- Gaisina L. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut NATIONALLICENCE 700 1- Strunskaya E. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut NATIONALLICENCE 700 1- Azancheev N. A. E. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center of the Russian Academy of Sciences, 8 ul. Akad. Arbuzova, 420083, Kazan, Russian Federation aut NATIONALLICENCE 773 0- Russian Chemical Bulletin Kluwer Academic Publishers-Plenum Publishers 49/2(2000-02-01), 310-313 1066-5285 49:2<310 2000 49 11172 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer