caa a22 4500 475844203 CHVBK 20180406123909.0 cr unu---uuuuu 170329e20000801xx s 000 0 eng 10.1023/A:1009030232453 doi (NATIONALLICENCE)springer-10.1023/A:1009030232453 Parallel synthesis and fast screening of heterogeneous catalysts [Elektronische Daten] [U. Rodemerck, P. Ignaszewski, M. Lucas, P. Claus, M. Baerns] We are presenting an effective method to prepare and test heterogeneous catalysts much faster than by the conventional way. A catalyst array was prepared via an incipient wetness method by combination of different amounts of Pt, Zr, and V on Al2O3 by means of an automatic liquid handler. For catalytic testing for methane oxidation a ceramic monolith reactor module, the channels of which contain the different catalyst compositions, was developed in which up to 250 catalyst compositions can be prepared and tested in parallel. Gas samples from each channel of the monolith were analysed sequentially by a mass spectrometer by moving the QMS inlet capillary into the channels using a three-dimensional positioning system which works at high temperatures. By comparison of the testing results with experiments carried out in flow reactors it is shown that the monolithic reactor is an efficient tool for fast screening of heterogeneous catalysts. Kluwer Academic Publishers, 2000 high throughput screening nationallicence combinatorial chemistry nationallicence heterogeneous catalysis nationallicence Rodemerck U. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut Ignaszewski P. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut Lucas M. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut Claus P. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut Baerns M. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut Topics in Catalysis Kluwer Academic Publishers-Plenum Publishers 13/3(2000-08-01), 249-252 1022-5528 13:3<249 2000 13 11244 https://doi.org/10.1023/A:1009030232453 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1023/A:1009030232453 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Rodemerck U. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut NATIONALLICENCE 700 1- Ignaszewski P. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut NATIONALLICENCE 700 1- Lucas M. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut NATIONALLICENCE 700 1- Claus P. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut NATIONALLICENCE 700 1- Baerns M. Institut für Angewandte Chemie Berlin-Adlershof e.V., Richard-Willstätter-Strasse 12, D-12489, Berlin, Germany aut NATIONALLICENCE 773 0- Topics in Catalysis Kluwer Academic Publishers-Plenum Publishers 13/3(2000-08-01), 249-252 1022-5528 13:3<249 2000 13 11244 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer