naa a22 4500 510804918 CHVBK 20180411083412.0 cr unu---uuuuu 180411e20130201xx s 000 0 eng 10.1007/s11664-012-2185-4 doi (NATIONALLICENCE)springer-10.1007/s11664-012-2185-4 Micro- and Nanostructure of Zn Whiskers and Their Coating [Elektronische Daten] [A. Etienne, E. Cadel, A. Lina, L. Cretinon, P. Pareige] To understand the mechanisms at the origin of whisker formation and growth, a Zn-electroplated steel prone to whiskering was studied. Several samples were prepared from different locations of the electroplated plate. Care was taken to extract samples at the root, in the nodule, or away from whiskers. Samples were characterized using electron backscattered diffraction (EBSD). Crystallographic data from EBSD show that recrystallized regions are present at the root of whiskers and in their nodules. These observations support whisker growth models based on recrystallization. In addition, atom probe tomography samples were prepared in the center of whiskers. The distribution of Zn atoms is almost homogeneous and no impurities are present in the whiskers. TMS, 2012 Electroplating nationallicence whiskers nationallicence electron scattering diffraction nationallicence recrystallization nationallicence focused ion beam nationallicence atom probe tomography nationallicence Etienne A. Groupe de Physique des Matériaux, Université et INSA de Rouen, UMR CNRS 6634, Avenue de l'Université BP 12, 76801, Saint Etienne du Rouvray Cedex, France aut Cadel E. Groupe de Physique des Matériaux, Université et INSA de Rouen, UMR CNRS 6634, Avenue de l'Université BP 12, 76801, Saint Etienne du Rouvray Cedex, France aut Lina A. Department Material and Mechanic Components, Corrosion Studies Laboratory, EDF R&D, 77818, Moret sur Loing Cedex, France aut Cretinon L. Department Electrical Equipment Laboratory, EDF R&D, 77818, Moret sur LoingCedex, France aut Pareige P. Groupe de Physique des Matériaux, Université et INSA de Rouen, UMR CNRS 6634, Avenue de l'Université BP 12, 76801, Saint Etienne du Rouvray Cedex, France aut Journal of Electronic Materials Springer US; http://www.springer-ny.com 42/2(2013-02-01), 272-279 0361-5235 42:2<272 2013 42 11664 https://doi.org/10.1007/s11664-012-2185-4 text/html Onlinezugriff via DOI 1 research-article jats NATIONALLICENCE 856 40 https://doi.org/10.1007/s11664-012-2185-4 text/html Onlinezugriff via DOI NATIONALLICENCE 700 1- Etienne A. Groupe de Physique des Matériaux, Université et INSA de Rouen, UMR CNRS 6634, Avenue de l'Université BP 12, 76801, Saint Etienne du Rouvray Cedex, France aut NATIONALLICENCE 700 1- Cadel E. Groupe de Physique des Matériaux, Université et INSA de Rouen, UMR CNRS 6634, Avenue de l'Université BP 12, 76801, Saint Etienne du Rouvray Cedex, France aut NATIONALLICENCE 700 1- Lina A. Department Material and Mechanic Components, Corrosion Studies Laboratory, EDF R&D, 77818, Moret sur Loing Cedex, France aut NATIONALLICENCE 700 1- Cretinon L. Department Electrical Equipment Laboratory, EDF R&D, 77818, Moret sur LoingCedex, France aut NATIONALLICENCE 700 1- Pareige P. Groupe de Physique des Matériaux, Université et INSA de Rouen, UMR CNRS 6634, Avenue de l'Université BP 12, 76801, Saint Etienne du Rouvray Cedex, France aut NATIONALLICENCE 773 0- Journal of Electronic Materials Springer US; http://www.springer-ny.com 42/2(2013-02-01), 272-279 0361-5235 42:2<272 2013 42 11664 Metadata rights reserved Springer special CC-BY-NC licence nationallicence BK010053 XK010053 XK010000 NATIONALLICENCE NATIONALLICENCE NL-springer