Method validation and quality assurance of an ICP-MS protocol for the evaluation of trace and major elements in ambient aerosol samples and application to an air quality surveillance network

Verfasser / Beitragende:
[M. Palomo-Marín, E. Pinilla-Gil, L. Calvo-Blázquez, X. Querol-Carceller]
Ort, Verlag, Jahr:
2015
Enthalten in:
Accreditation and Quality Assurance, 20/1(2015-02-01), 17-23
Format:
Artikel (online)
ID: 605465487
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024 7 0 |a 10.1007/s00769-014-1099-7  |2 doi 
035 |a (NATIONALLICENCE)springer-10.1007/s00769-014-1099-7 
245 0 0 |a Method validation and quality assurance of an ICP-MS protocol for the evaluation of trace and major elements in ambient aerosol samples and application to an air quality surveillance network  |h [Elektronische Daten]  |c [M. Palomo-Marín, E. Pinilla-Gil, L. Calvo-Blázquez, X. Querol-Carceller] 
520 3 |a This study presents the results of a quality assurance evaluation program applied to the method routinely used for the evaluation of a large elemental profile in aerosol samples from the air quality surveillance network of Extremadura, Spain, where low pollution levels are usually encountered. A critical evaluation of the most relevant analytical steps is presented, including long-term blank values evaluation, limits of detection, certified reference material recoveries, method uncertainty and results of comparison studies for gravimetric and trace element analysis. Results obtained at the air quality network of Extremadura for the gravimetric and multielemental analysis are presented for the 2008 campaign. 
540 |a Springer-Verlag Berlin Heidelberg, 2014 
690 7 |a Quality assurance  |2 nationallicence 
690 7 |a Ambient aerosol  |2 nationallicence 
690 7 |a Elemental profile  |2 nationallicence 
690 7 |a ICP-MS  |2 nationallicence 
700 1 |a Palomo-Marín  |D M.  |u Department of Analytical Chemistry, University of Extremadura, Av. de Elvas, s/n, 06006, Badajoz, Spain  |4 aut 
700 1 |a Pinilla-Gil  |D E.  |u Department of Analytical Chemistry, University of Extremadura, Av. de Elvas, s/n, 06006, Badajoz, Spain  |4 aut 
700 1 |a Calvo-Blázquez  |D L.  |u Department of Analytical Chemistry, University of Extremadura, Av. de Elvas, s/n, 06006, Badajoz, Spain  |4 aut 
700 1 |a Querol-Carceller  |D X.  |u Institute of Environmental Assessment and Water Research, IDÆA, CSIC, C/Lluís Solé y Sabarís S/N, 08028, Barcelona, Spain  |4 aut 
773 0 |t Accreditation and Quality Assurance  |d Springer Berlin Heidelberg  |g 20/1(2015-02-01), 17-23  |x 0949-1775  |q 20:1<17  |1 2015  |2 20  |o 769 
856 4 0 |u https://doi.org/10.1007/s00769-014-1099-7  |q text/html  |z Onlinezugriff via DOI 
898 |a BK010053  |b XK010053  |c XK010000 
900 7 |a Metadata rights reserved  |b Springer special CC-BY-NC licence  |2 nationallicence 
908 |D 1  |a research-article  |2 jats 
949 |B NATIONALLICENCE  |F NATIONALLICENCE  |b NL-springer 
950 |B NATIONALLICENCE  |P 856  |E 40  |u https://doi.org/10.1007/s00769-014-1099-7  |q text/html  |z Onlinezugriff via DOI 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Palomo-Marín  |D M.  |u Department of Analytical Chemistry, University of Extremadura, Av. de Elvas, s/n, 06006, Badajoz, Spain  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Pinilla-Gil  |D E.  |u Department of Analytical Chemistry, University of Extremadura, Av. de Elvas, s/n, 06006, Badajoz, Spain  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Calvo-Blázquez  |D L.  |u Department of Analytical Chemistry, University of Extremadura, Av. de Elvas, s/n, 06006, Badajoz, Spain  |4 aut 
950 |B NATIONALLICENCE  |P 700  |E 1-  |a Querol-Carceller  |D X.  |u Institute of Environmental Assessment and Water Research, IDÆA, CSIC, C/Lluís Solé y Sabarís S/N, 08028, Barcelona, Spain  |4 aut 
950 |B NATIONALLICENCE  |P 773  |E 0-  |t Accreditation and Quality Assurance  |d Springer Berlin Heidelberg  |g 20/1(2015-02-01), 17-23  |x 0949-1775  |q 20:1<17  |1 2015  |2 20  |o 769